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1.
Isoko Takahashi Takanori Sugimoto Yasuo Takasu Mariko Yamasaki Yasutoshi Sasaki Youji Kikata 《Wood Science and Technology》2012,46(1-3):419-429
The thermoplastic flow behavior of cedar flour steamed at different temperatures in the range of 160–220°C was measured using a rheometer and compared with that of beech flour. The temperature at which the cedar flour starts to flow was approximately 70°C higher than that of beech flour, and the cedar flour exhibited low flowability. Furthermore, thermoplastic moldings were prepared from cedar and beech flours, and their physical properties were examined. Similar to the case of beech, a resin-like molding with a density of approximately 1.45?g/cm3 was obtained from the cedar flour steamed at 180°C or higher, and it was revealed by SEM observation that in these moldings wood flour particles adhere to each other. The specific bending strength was maximum for the moldings obtained from 180°C-steamed flour for both types of wood. 相似文献
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3.
The effect of heating on the hygroscopicity of Japanese cedar wood was investigated as a simple evaluation of thermal degradation
in large-dimension timber being kiln-dried at high temperatures (>100°C). Small wood pieces were heated at 120°C in the absence
of moisture (dry heating) and steamed at 60°, 90°, and 120°C with saturated water vapor over 2 weeks, and their equilibrium
moisture contents (M) at 20°C and 60% relative humidity (RH) were compared with those of unheated samples. No significant change was induced by
steaming at 60°C, while heating above 90°C caused loss in weight (WL) and reduction in M of wood. The effects of steaming were greater than those of dry heating at the same heating temperature. After extraction
in water, the steamed wood showed additional WL and slight increase in M because of the loss of water-soluble decomposition residue. The M of heated wood decreased with increasing WL, and such a correlation became clearer after the extraction in water. On the basis of experimental correlation, the WL of local parts in large-dimension kiln-dried timber was evaluated from their M values. The results indicated that the thermal degradation of inner parts was greater than that of outer parts. 相似文献
4.
Eiichi Obataya Sakae Shibutani Kensuke Hanata Shuichi Doi 《Journal of Wood Science》2006,52(2):111-114
Japanese cedar wood specimens were steamed at 80°, 100°, and 120°C over 14 days, and their equilibrium moisture content (M)
at 20°C and 60% relative humidity, longitudinal dynamic Young’s modulus (E), bending strength (σ
max), and breaking strain (ε
max) were compared with those of unheated specimens. Steaming for a longer duration at a higher temperature resulted in a greater
reduction in M, σ
max, and ε
max. The E of wood was slightly enhanced by steaming at 100°C for 1–4 days and 120°C for 1–2 days, and thereafter it decreased. The
slight increase in the E of sapwood was attributable to the reduction in hygroscopicity, while sufficient explanation was not given for a greater
increase in the heartwood stiffness. Irrespective of the steaming temperature, the correlations between M and the mechanical properties of steamed wood were expressed in terms of simple curves. M values above 8% indicated a slight reduction in E and s max, whereas M values below 8% indicated a marked decrease in the mechanical performances. In addition, the e max decreased almost linearly
with a decrease in the value of M. These results suggest that hygroscopicity measurement enables the evaluation of degradation in the mechanical performances
of wood caused by steaming at high temperatures. 相似文献
5.
Method for measuring viscoelastic properties of wood under high temperature and high pressure steam conditions 总被引：3，自引：0，他引：3
A method for measuring the viscoelastic properties of wood under high temperature and high pressure steam was developed using a testing machine with a built-in autoclave. A newly developed load cell capable of resisting a steam pressure of 16kgf/cm2 and a temperature of 200°C was installed in the autoclave. This load cell could be used to determine precisely the loads while steaming at temperatures from 100°C to 200°C. In addition to load-detection problems, it was necessary to avoid the nonuniform thermal degradation of wood during the measurement process under steaming at high temperatures. This nonuniform degradation could be minimized by shortening the time required for the wood to attain thermal equilibrium using specimens conditioned to the fiber saturation point. According to this method, a stress relaxation curve for sugi (Cryptomeria japonica D. Don) wood being compressed while steaming at 180°C was obtained. The stress was seen to decrease rapidly with time, reaching almost zero at 3000s. 相似文献
6.
以淀粉和木粉为原料,甘油为增塑剂,通过挤出成型制备淀粉/木粉可生物降解复合材料,重点研究淀粉/木粉混合比例对复合材料性能的影响。采用扫描电镜（SEM）、X射线衍射仪（XRD）和热重分析（TGA）对复合材料进行表征,并对复合材料的力学性能和吸水性能进行测试。实验结果表明：木粉的加入破坏热塑性淀粉的连续性,使复合材料的结晶度增大。复合材料的拉伸强度、吸水率和吸水厚度膨胀率随着木粉比例增大逐渐增大,断裂伸长率却逐渐降低。TGA测试结果表明,随着木粉加入比例增大,复合材料的热分解起始温度逐渐降低,但热分解的终止温度逐渐升高,淀粉和木粉两相依赖性逐渐减弱。 相似文献
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8.
Masahiro Takatani Osamu Kato Takashi Kitayama Tadashi Okamoto Mitsuhiko Tanahashi 《Journal of Wood Science》2000,46(3):210-214
The effect of steam-exploded wood flour (SE) added to wood flour/plastic composite was examined using SE from beech, Japanese cedar, and red meranti and three kinds of thermoplastic polymer: polymethylmethacrylate, polyvinyl chloride, and polystyrene. Addition of SE increased the fracture strength and water resistance of the composite board to an extent dependent on the polymer species and the composition of wood/SE/polymer. However, water resistance decreased with the increasing proportion of SE when SE meranti was added. Effects of the wood species of SE on the properties of resulting board were small. An increased moisture content of wood flour or SE (or both) increased the variation of board performance. 相似文献
9.
木材干燥过程中,介质循环速度是一个影响木材干燥的重要工艺参数.在木材各含水率阶段,通过试验分析研究不同介质循环速度对木材干燥速度的影响.结果表明,介质循环速度对干燥速度的影响显著,但其影响随木材含水率（MC）的降低而减弱.在低介质循环速度条件下,试件MC大于45％时,表现为木材干燥速度和木材含水率偏差（△MC）随循环风速的增加而增加,呈显著正相关关系;试件MC介于35％ ～ 45％之间时,正相关关系存在但不显著;试件MC小于35％时,干燥室内循环风速的大小不影响木材的干燥速度和木材含水率偏差（△MC）.对试件表层含水率分析,试件表层含水率大于25％时,试件表面循环风速对试件表层含水率的影响显著;试件表层含水率小于25％时,试件表面循环风速对试件表层含水率的影响很小,不同循环风速下试件表层含水率基本一样. 相似文献
10.
Luigi Todaro Roberto Zanuttini Antonio Scopa Nicola Moretti 《Wood Science and Technology》2012,46(1-3):563-578
A combined effect of steaming and heat treatment was imposed on green Turkey oak wood, both for sapwood and heartwood. Steaming was carried out in an autoclave at 100–120–130°C whereas heating was carried out in an oven for 2?h at 120–180°C. Equilibrium moisture content at dry, intermediate and moist state both in desorption and adsorption, swelling, cup, twist, color change, and spectral reflectance measures were registered. Swelling and water absorption decreased due to the hydro-thermal treatment. During adsorption, heartwood showed a higher hygroscopic inertia compared to sapwood and this difference increased with temperature. Cup increased with temperature in the steaming process. Twist seemed to be affected more by quality of original trunks than treatments. The wood color was more sensitive at a steaming temperature of 130°C combined with heat treatment at 180°C. Transitional treatments assured more reliable results on homogenization of hue between sapwood and heartwood. 相似文献
11.
Tsunehisa Miki Hiroyuki Sugimoto Keisuke Kojiro Yuzo Furuta Kozo Kanayama 《Journal of Wood Science》2012,58(4):300-308
The thermal properties and transitions of solid and ground wood samples conditioned at different humidity conditions were investigated by temperature-modulated differential scanning calorimetry. A time-dependent transition was detected as an endothermic peak in the total and non-reversing heat flows and as a step change in the reversing heat flow during the first heating run of samples with moisture contents above 5?%, but it disappeared in the second heating run. These different thermal behaviors indicate that the effect of heat and moisture on the thermal properties of wood is history dependent. This step change in the reversing heat flow is considered to be a glass transition of moist wood. Other relaxation processes (e.g., enthalpy relaxation) occur simultaneously with this glass transition. The temperature ranges of the transition and the relaxation decreased drastically as the moisture content increased up to 11?%, while they remained almost constant at higher moisture contents. In addition, the transitions of the ground wood occurred at lower temperatures than those of the solid wood at similar moisture contents. Kissinger plots revealed that the apparent activation energy for the glass transition of the solid wood with a moisture content of 11?% was about 600?kJ/mol, whereas that of the ground wood was 220?kJ/mol. 相似文献
12.
Compression of wood under saturated steam, superheated steam, and transient conditions at 150°C, 160°C, and 170°C 总被引：1，自引：1，他引：0
In this paper, the compressive deformation of hybrid poplar wood (Populus deltoides?×?Populus trichocarpa) at high temperature (150, 160, and 170°C) and under various conditions of steam pressure was studied. Temperature and conditions of steam environment affected the relative density change and creep deformation during compression, as well as properties of the resulting densified material. While the temperature significantly affected the compression deformation of specimens compressed under transient and superheated steam conditions, temperature within the range studied had little effect on the compressive deformation in saturated steam. In all tested conditions, compression deformation was achieved without cell wall fractures. Higher temperature of compression, regardless of steam condition, resulted in lower equilibrium moisture content. In specimens compressed under saturated steam, the modulus of rupture (MOR) and modulus of elasticity (MOE) were increased proportionally to the increase in density, while the compression under superheated steam produced lower increase in the MOE and MOR than expected based on the increase in density. Compression in transient steam conditions at 170°C produced densified wood with higher MOE and MOR than expected based on the increase in density. 相似文献
13.
Claude Feldman Pambou Nziengui Samuel Ikogou 《Wood material science & engineering》2018,13(4):190-196
The mechanical behavior of Aucoumea Klaineana Pierre (AKP) under progressive static and cyclic compressive loading at various moisture content (MC) stages is investigated herein. This tropical species, also called Okume, originates from the Congo Basin, particularly Gabon. The experimental device used is composed of an electronic testing machine, a system yielding the corresponding MC, and AKP wood samples. In all, 15 AKP samples were loaded in statics, at different MC levels, until the first cracks led to characterizing the mechanical behavior of the species in static compression along the longitudinal direction. Next, seven samples of AKP were gradually loaded at distinct MC values, with five under cyclic longitudinal compression. Results show that under a static longitudinal compressive loading, the modulus of elasticity (MOE) of AKP decreases as sample MC increases. For the cyclic compressive loading after the first cycle, sample MOE increases with both the intensity and number of loading cycles as well as with the permanent deformation of each cycle. Moreover, it can be observed that within the plasticity domain, the impact of MC variation on the mechanical behavior of AKP is negligible. 相似文献
14.
前处理方法对杨木木粉改性反应以及改性木粉热流动性的影响 总被引：2，自引：0，他引：2
研究了几种前处理方法对杨木木粉的改性反应和改性杨木木粉热流动性、溶解性的影响。发现加热预处理和饱和氯水前处理都会使木素的三维结构产生变化，从而使羟乙基化木粉产生热流动性，同时也降低了苄基化木粉的粘流温度（Ｔｆ０。几种前处理方法也使改性木粉在某些溶剂中的溶解度有不同程度的提高。 相似文献
15.
A new method for monitoring moisture content during radio-frequency (RF)/vacuum drying was developed by measurement of temperature
and pressure in wood. Temperature and pressure inside the wood were measured simultaneously during RF/vacuum drying at the
same point. The relative humidity (RH) and moisture content (MC) below the fiber saturation point (FSP) were calculated based
on temperature and pressure, and the relationship between the temperature, RH, and equilibrium moisture content (EMC) at the
measurement point. When the moisture content was below the FSP, the calculated MC was slightly greater than the value given
by oven drying. The absolute error was within 0.8% near the open cross side, and was within 1.8% at another measurement point.
Thus, we concluded that it was practicable to monitor the moisture content below the FSP according to the temperature and
pressure inside the wood.
Part of this study was presented at the 15th Annual Meeting of the Chugoku Shikoku Branch of the Japan Wood Research Society,
Higashi-Hiroshima, Japan, September 2003 相似文献
16.
Compression creep experiments of Douglas-fir wood (Pseudotsuga menziesii) were performed at high temperature (150°C, 160°C, and 170°C) and under various conditions of steam pressure. The results established that environment conditions had a significant effect on compressive deformation, with the largest deformation obtained under saturated steam conditions. While the temperature significantly affected the compressive deformation of specimens under transient conditions, the temperature within the range studied had little effect on the compressive deformation in saturated steam. Furthermore, in specimens compressed under superheated and transient steam conditions, primary creep behavior was exhibited; while in specimens compressed under saturated steam conditions, creep deformation appeared to enter directly into secondary creep. Moreover, in saturated steam specimens very little creep was observed due to high initial deformation and little potential for additional cell wall buckling. The compressive creep measurements of Douglas-fir were compared with compressive creep of hybrid poplar (Populus deltoides × Populus trichocarpa). Due to lower initial density, and perhaps smaller microfiber angle and lower lignin content of tension wood, the compressive creep modulus of hybrid poplar was lower than Douglas-fir. Therefore, compressive deformation of Douglas-fir, at nearly all examined steam conditions and temperatures, was smaller than compressive deformation of hybrid poplar. 相似文献
17.
Wim Willems 《Wood Science and Technology》2014,48(3):483-498
By expressing wood moisture content data as a function of adsorption energy, an interesting scaling capability is obtained, wherefrom the general hydrostatic pressure and temperature dependence of wood moisture content is determined. The scaling law is fully consistent with the thermodynamics of swelling. It can be used to transform room condition sorption isotherms to other temperatures and hydrostatic pressures, provided that the wood matrix is not irreversibly modified. A special procedure is suggested for the case of an irreversibly changing wood matrix, as in thermal modification and thermo-hydro-mechanical treatments. Using the present scaling theory, several fundamental aspects of wood moisture sorption are explained, such as the absence of a significant quantity of strongly bound wood moisture, the internal stress generation by sorption hysteresis in the wood cell wall, and the reason for the reversible disappearance of the sigmoid shape of the sorption isotherm at higher temperature. The results of this research may be useful (a) for transformation of known sorption data to other conditions, notably where in situ moisture measurements are difficult to perform and (b) to quantify the effects of internal stresses in the ultrastructure of the cell wall on moisture content. 相似文献
18.
In order to analyze the effect of temperature gradient on moisture movement during highly intensive drying, such as microwave-vacuum
drying, the profile of the temperature and moisture content in sealed wood whose opposite faces were subjected to temperature
gradient for a short time was measured. The ratio of the moisture content (MC) gradient to the temperature gradient (dM/dT) was calculated and the factors influencing moisture movement under nonisothermal conditions were discussed. The results
indicate that moisture moved in wood from the warm surface to the cold one even if opposite faces of the sealed wood assembly
were exposed continuously to different but constant temperatures for a short period. The moisture content on the cold surface
was higher than that on the warm surface. The moisture content gradient opposite to the temperature gradient was established,
and the dM/dT was below 0.9%/°C. The temperature in the sample and the distance from the hot surface of the sample was strongly linearly
correlated. With an increase in temperature, initial moisture content and experimental time, the dM/dT was significantly increased.
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Translated from Journal of Beijing Forestry University, 2005, 27(2): 96–100 [译自: 北京林业大学学报, 2005, 27(2): 96–100] 相似文献
19.
Li Xian-jun Zhang Bi-guang Li Wen-jun 《中国林学(英文版)》2005,7(2):47-51
In order to analyze the effects of the temperature gradient on moisture movement during the highly intensive microwave-vacuum drying, thermal diffusion of Masson pine wood was studied. Internal distribution of temperature and moisture in Masson pine samples sealed by epoxy resin and aluminum foil was measured, the magnitude of thermal diffusion was calculated and the influencing factors of thermal diffusion were discussed. Results showed that with the transfer of moisture toward the low temperature in wood, opposite temperature and moisture gradient occurred. The initial moisture content （MC）, temperature and time are important factors affecting this process; the thermal diffusion is in proportion to wood temperature, its initial moisture and time. The temperature and distance from hot surface is strongly linearly correlated, and the relationship between MCs at different locations and distance from the hot end surface changes from logarithmically form to exponentially form with the increase in experimental time. 相似文献
20.
To improve interfacial adhesion between wood veneer and high-density polyethylene (HDPE) film, wood veneer was thermally modified in an oven or chemically modified by vinyltrimethoxysilane. The wood veneers were used to prepare plastic-bonded wood composites (PBWC) in a flat-press process using HDPE films as adhesives. The results showed that both modifications reduced veneer hydrophilicity and led to enhancement in shear strength, wood failure, and water resistance of the resulting PBWC. The thermal treatment significantly decreased the storage modulus close to 130 °C (the melting temperature of plastic). Thermal-treated wood veneer maintains mechanical interlocking for bonding and veneer strength which then declined under thermal treatment due to hemicellulose degradation and cellulose de-polymerization. In the silane-treated PBWC, enhanced interlocking and a stronger bonding structure resulted from the reaction between the silane-treated veneer and HDPE. This strong bonding structure allowed thermal stability improvement demonstrated by high modulus and low tanδ values. However, the strength of silane-treated PBWC was still much lower than thermosetting resin-bonded composites at higher temperatures due to the melting behavior of thermoplastic polymer, precluding its use in certain applications. 相似文献