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1.
The aim of this work was to study the effects of extrusion barrel temperature (75–140°C) and feed moisture (16–30%) on the production of third‐generation snacks expanded by microwave heating. A blend of potato starch (50%), quality protein maize (QPM) (35%), and soybean meal (SM) (15%) was used in the preparation of the snacks. A laboratory single extruder with a 1.5 × 20.0 × 100 mm die‐nozzle and a central composite routable experimental design were used. Expansion index (EI) and bulk density (BD) were measured in expanded pellets, viscosity at 83°C (V83), thermal properties, and relative crystallinity were measured in extruded pellets. EI increased and BD decreased when the barrel temperature was increased, while the feed moisture effect was not significant. V83 increased when feed moisture increased. Extrusion modified the crystalline structures of the pellets and the X‐ray data suggests the formation of new structures, probably due to the development of amylose‐lipid complexes. The maximum expansion of pellets was found at barrel temperatures of 123–140°C, and feed moisture of 24.5–30%. It is possible to obtain a functional third‐generation snack with good expansion characteristics using a microwave oven, and this snack has health benefits due to the addition of QPM and SM.  相似文献   

2.
The microwave expansion of glassy, unexpanded amylopectin pellets was studied. Amylopectin was extruded at three levels of specific mechanical energy (483, 809, and 846 kJ/kg), and 35–40% moisture content, without expansion at the die. Glassy pellets were obtained by drying and equilibrating the extrudates at five water activities (aw 0, 0.11, 0.33, 0.67, and 0.75). The pellets were characterized by measuring volume, porosity, and moisture content. The pellets were then expanded in a constant power microwave oven to determine the degree of expansion. When subjected to microwave heating, regardless of extrusion condition and initial aw, the pellets expanded from the center where the highest temperature was recorded and then expansion advanced in the whole volume. Maximum expansion was reached after 30 sec of heating, after which samples started to burn from the center. Samples simultaneously expanded and lost moisture, both processes being faster and more intense for pellets of higher initial aw. No expansion was observed for the pellets stored at aw 0, while collapse was observed for pellets stored at aw 0.73. A linear correlation between pellet expansion temperature and glass transition temperature was obtained. A hypothesis for the microwave expansion of glassy extrudates was formulated and represented on a state diagram.  相似文献   

3.
Extruded pellets were prepared from normal corn starch using a corotating twin‐screw extruder (25:1 L/D ratio, 31 mm diameter screw), and then expanded by heating in a conventional microwave oven for 70 sec. The effects of gelatinization level and moisture content of the extruded pellets on the morphology and physical properties of the microwave‐expanded products such as puffing efficiency, expansion bulk volume, and bulk density were investigated. The expanded shape and air cell structure differed according to the degree of gelatinization of the pellets. Maximum puffing efficiency and expansion volume with the pellets containing 11% moisture were achieved at 52% gelatinization. For this level of gelatinization, starch was extruded at 90°C barrel temperature. In addition, the moisture content of the pellets critically affected the expansion behavior. The maximum puffing efficiency and expansion volume were achieved in a moisture range of 10~13%. For optimum product shape and uniform air cell distribution, the pellets should undergo sudden release of the superheated vapor during the microwave‐heating. The expansion by microwave‐heating was optimized at ≈50% gelatinization.  相似文献   

4.
The effect of solid fat (melting point 70°C) and liquid fat (melting point ‐20°C) on the microwave expansion of extruded glassy amylopectin pellets was investigated. Glassy, unexpanded amylopectin extrudates containing ≤10% fat were equilibrated at different water activity levels (aw) and then expanded by microwave heating. Expanded products were characterized by analyzing degree of expansion, structure, and texture. For the aw range studied, expansion increased with increasing aw of the pellets until a maximum at aw = 0.605 and then decreased. Completely dehydrated samples did not expand at all. This demonstrated that moisture was the driving force in the microwave expansion of the pellets. The addition of solid fat contributed greatly to expansion. The highest degree of expansion was obtained for pellets containing 6% solid fat at all aw levels. Due to the effect on expansion, the addition of solid fat also affected the microstructure and texture of the expanded products. Concentrations of solid fat >2% resulted in expanded products with a large number of cells, uniform in size, with thin cell walls. Liquid fat addition had a negative effect on microwave expansion. The expanded products obtained from pellets that contained liquid fat had a lower expansion volume and a coarser structure.  相似文献   

5.
In various Latin American countries, large volumes of potato are classified as unsuitable for use as food and destined for use as feed. This raw material has a high starch and fiber content that could be used in the production of different kinds of food. The objective of this research was the preparation and characterization of extruded whole potato pellets expanded by microwave heating. A 33 central composite routable experimental design and response surface methodology were used. The barrel temperature (BT, 93–127°C), feed moisture (FM, 19–29%), and corn starch concentration (CS, 3–37%) in the blends were evaluated. CS was the most important variable affecting the functional properties of the expanded pellets. Adding CS to the blends increased the expansion index and viscosity and improved luminosity, decreasing the apparent density and breaking force of the products. Low BT and especially high FM increased the luminosity of the expanded pellets. Increasing FM content increased the viscosity of the expanded pellets. The best functional characteristics for the expanded pellets were obtained using a blend of 63% potato flour and 37% CS, extruded at 110°C BT with 24% FM content. Nonfood-grade whole potato flour showed good potential for use in the production of expanded pellets with acceptable functional properties.  相似文献   

6.
Extrusion with CO2 injection was developed to simplify the process of producing vacuum‐puffed yukwa (rice snacks). The effects of feed moisture content and CO2 injection on the characteristics of extruded pellets (maximum viscosity and degree of gelatinization) and vacuum‐puffed yukwa (expansion ratio, bulk density, hardness, and color) were investigated. Higher feed moisture increased the size of vacuum‐puffed yukwa and the degree of gelatinization, whereas the maximum viscosity decreased. Maximum viscosity and gelatinization degree of extruded pellets were highly correlated with expansion ratio, bulk density, hardness, and color values of vacuum‐puffed yukwa. Increasing feed moisture content significantly increased expansion ratio but decreased bulk density and hardness. CO2 injection decreased bulk density and hardness of vacuum‐puffed yukwa.  相似文献   

7.
Carboxymethyl cellulose (CMC) is added to tortillas to maintain a pliable texture during storage. A need exists to optimize or replace CMC in masa and tortilla manufacturing with cheaper yet adequate alternatives. Change in water distribution upon gum addition may be key to understanding stability of cooked masa. Therefore, the objective of this study was to characterize the state and distribution of water in masa systems containing two types of CMC and guar gum. Masa was mixed with 10% (1% in viscosity measurements) of different gums (either one of two CMCs varying in viscosity or guar) then hydrated to 50% moisture content. Viscosity, water holding capacity (WHC), total moisture content (TGA) as well as “freezable” (FW) and “unfreezable” (UFW) water (DSC) of all samples were obtained and compared. Viscosity measurements indicated guar gum may provide a good substitution for high viscosity CMC. The two water measurements, WHC and UFW, differed as to the effect of viscosity on water entrapment. WHC represented the short‐term imbibing of gums, while UFW indicated how the hydrocolloids responded in masa given full hydration time. UFW in guar gum was lower than in medium viscosity CMC. These initial results indicate that guar gum may prove a good substitute for CMC in masa applications.  相似文献   

8.
Disadvantages of frozen doughs are their variable performance and loss of stability over long‐term frozen storage. Changes in rheological properties of frozen doughs have been reported to be due to the physical damage of the gluten network caused by ice crystallization and recrystallization. The objective of this study was to determine the effect of hydrophilic gums on ice crystallization and recrystallization for improvement of the shelf‐life stability of frozen dough. The present research involved use of the Hard Red Spring wheat cultivar Grandin and hydrophilic gums such as carboxymethyl cellulose (CMC), gum arabic, kappa carrageenan (κ‐carrageenan), and locust bean gum at three different levels each on doughs stored frozen for up to 16 weeks. The dough characteristics were analyzed after day 0, day 1, and after 4, 8, 12, and 16 weeks of frozen storage using data from differential scanning calorimetry (DSC), water activity, extensigraph, and proof time. The ΔH value of freezable water endothermic transitions obtained using DSC increased with storage time for all treatments. However, addition of different levels of the four gums lowered the ΔH value, indicating a decrease in freezable water. Doughs with locust bean gum gave a higher peak force, measured using the Kieffer dough extensibility rig of the texture analyzer, and lower proof time, indicating better retention of baking quality. Maximum resistance to extension increased upon addition of 1 and 3%; CMC; 1 and 3%; κ‐carrageenan; and 1, 2, and 3% locust bean gum as compared with the control. The various periods of storage or gum treatments did not affect the water activity of the thawed frozen doughs. Doughs with locust bean gum gave significantly lower proof time compared with the other treatments and the control. CMC gave the second lowest values, followed by gum arabic treatment. Addition of κ‐carrageenan increased the proof time compared with the control. In summary, locust bean gum, gum arabic, and CMC improved the dough characteristics to varying degrees. κ‐Carrageenan was the only gum that showed a detrimental effect on frozen dough.  相似文献   

9.
The aim of this work was to study the effects of barrel temperature (BT, 93.5–140.5°C), feed moisture (FM, 21.3–34.7%), and winter squash flour content (SFC, 0.43–15.6%) on physicochemical properties of microwave‐expanded third‐generation snack foods obtained by extrusion. Physicochemical properties used for optimization were expansion index (EI), penetration force (PF), specific mechanical energy (SME), and total color difference (ΔE). Response surface methodology was used for the analysis of data. The highest values of EI and lowest values of PF were found at high BT and low FM. The lowest values of SME were obtained at high levels of FM throughout the range of BT and SFC, whereas the highest values of ΔE were obtained at high SFC and low FM. Increasing levels of SFC increased ΔE values, whereas EI and SME values decreased. The best processing conditions (EI > 6.0, PF < 9.5 N, SME < 172 kJ/kg, and ΔE < 18) were found in the range of BT, 122–141°C; FM, 24.7–29.5%; and SFC, 0–10.9%. Under optimal process conditions, the retention of total carotenoids was higher than 60%. It is possible to manufacture third‐generation snack foods with good physicochemical properties, which could bring a health benefit because of the presence of carotenoids and dietary fiber in winter squash flour.  相似文献   

10.
Hydrophilic gums have been shown to improve the shelf‐life stability of frozen doughs during long periods of frozen storage. The objective of this research was to determine the effect of gums on starch and protein characteristics of frozen doughs using electron microscopy and electrophoresis studies. Frozen doughs, supplemented with three levels of gum arabic, carboxy methyl cellulose (CMC), kappa (κ) carrageenan, and locust bean gum, were studied after day 1 and after 4, 8, 12, and 16 weeks of frozen storage. Changes in the ultra structure of the frozen doughs were investigated, as well as the solubilities and composition of dough proteins by SDS‐PAGE. Scanning electron micrographs of doughs evaluated on day 0 (unfrozen) showed starch granules securely embedded in the gluten matrix. However, after 8 and 16 weeks of frozen storage, the frozen control dough without the gum additives clearly showed damage to the gluten network, and the starch granules appeared to be separated from the gluten. Doughs with locust bean gum and gum arabic showed better retention of the gluten network compared with the frozen control evaluated after different periods of storage. The SDS‐soluble protein content increased while residue protein content decreased as the frozen storage time increased. After each frozen storage period, the control dough without the gum additive had the highest amount of SDS‐soluble proteins and the lowest amount of residue proteins when compared with the doughs treated with gums. κ‐Carrageenan and locust bean gum had the lowest amount of SDS‐soluble proteins compared with doughs with CMC and gum arabic. The frozen control had the lowest amount of residue proteins at any particular time of frozen storage. κ‐Carrageenan treated doughs had the highest amount of residue proteins, followed by doughs with locust bean gum. Doughs with gum arabic and CMC had the lowest amount of residue proteins but still higher than the control doughs.  相似文献   

11.
The impact of extrusion on physical and sensory properties and on the in vitro bile acid (BA) binding was examined for N979 and Jim oat (Avena sativa) lines with 8.1 and 4.8% β‐glucan, respectively. Based on hardness and edibility of products made from Jim oats, moisture concentrations of 16–25% and temperatures of 165–180°C were selected for N979 extrusion. Jim‐based cereal had a significantly greater (P < 0.05) expansion ratio than did N979‐based cereal at most moistures. N979 cereal was browner, but not harder, than Jim cereal. Extruded products from N979 and Jim oats had 5.29–5.99% and 3.38–3.94% β‐glucan, respectively. Changing extrusion temperature or moisture content did not affect β‐glucan concentration in the products. N979 cereal made at 165°C and 16% moisture had greater BA binding than at other conditions, and had crunchiness comparable to cereals made at other conditions. BA binding of Cheerios brand breakfast cereal was close to that of N979 cereal made at 180°C and 18% moisture, but lower than cereals made at other conditions. Cereals made from Jim and N979 oats were browner, harder, coarser, and crunchier than Cheerios breakfast cereal. Proper processing and preparation techniques should be considered when producing extruded products from high β‐glucan oats.  相似文献   

12.
A phosphorylated cross‐linked type 4 resistant wheat starch (RS4) containing 85.5% total dietary fiber (TDF) replaced 5–20% of the whole corn flour in an extruded ring‐shaped ready‐to‐eat breakfast cereal formulation. TDF content of the dry ingredient blend increased by roughly 3.6% for every 5% of added RS4. TDF loss during extrusion processing increased as RS4 level increased; however, a high percentage (78–89%) of the TDF content was retained in the final product. Product density increased as level of RS4 increased, but no effect on the specific mechanical energy was observed. X‐ray microtomography showed that RS4 addition did not affect internal air‐cell wall thickness, air‐cell size, or porosity. Moreover, addition of 5 or 10% RS4 did not affect expansion, physical appearance, initial crispness, or bowl life of the cereal rings. High levels of RS4 (15 and 20%) decreased cereal ring diameter but increased initial (dry) product crispness and extended bowl life. In general, RS4 addition level did not affect moisture content or moisture uptake of cereal rings during soaking in milk. Furthermore, moisture content and moisture uptake did not appear to influence the crispness of milk‐soaked cereal rings.  相似文献   

13.
Waxy maize (native and hydroxypropylated [HP]) and potato starches were impregnated with ionic gums (sodium alginate, CMC, and xanthan, 1% based on starch solids) and heat‐treated in a dry state for 0, 2, or 4 hr at 130°C. Effects of the dry heating on paste viscosity (RVA) and clarity (light transmittance) were examined. Heat treatment with sodium alginate and CMC raised the paste viscosities of native and HP waxy maize starches, but decreased that of potato starch. Xanthan provided the most substantial changes in paste viscosity among the tested gums. It appeared to heavily restrict granule swelling of the waxy maize starches, but it increased swelling of potato starch granules. Dry heating raised the paste viscosity of all the starch‐gum mixtures tested, except the potato starchalginate mixture. The final viscosity at 50°C of a 7% paste was raised in all other starches by ≈500–1,000 cP by this treatment. The paste of waxy maize starch‐gum products became opaque and shorter textured by the heat treatment, regardless of the gum type, whereas potato starch‐gum products did not show any obvious change in paste clarity. Ionic gums could behave as cross‐linking agents as well as form graft copolymers through heatinduced ester formation. This simple heating process with ionic gums could be used as a modification method for starch.  相似文献   

14.
Extrudate expansion of cereal‐based products is largely dependent on the molecular interactions and structural transformations that proteins undergo during extrusion processing. Such changes strongly influence the characteristic rheological properties of the melt. It is possible to modify rheological properties of wheat flour during extrusion processing, in particular shear viscosity, with cysteine. The objective of this work was to further develop an understanding of the molecular interactions and structural transformations of wheat flour from dynamic oscillatory rheological measurements. Temperature and frequency sweeps were conducted in the linear viscoelastic range of the material. Changes in the storage modulus (G′), the loss modulus (G″) and the loss tangent (tan δ) of 25% moisture wheat flour disks as a function of cysteine concentration (0–0.75%) were monitored. Molecular weight between cross‐links (Mc) and the number of cross‐links (Nc) per glutenin molecule were determined from frequency sweep data. Increasing cysteine concentration broke cross‐links by decreasing G′ maximum and increasing tan δ values. Molecular weight between cross‐links increased and the number of cross‐links decreased. G′ values from temperature sweeps showed a similar trend. This information leads to a better understanding of the viscoelastic behavior of wheat flour doughs during extrusion cooking and elucidation of protein‐protein reaction mechanisms and other interactions in extruded cereal‐based snack foods.  相似文献   

15.
A heat expansion process similar to that used for expanded bead polystyrene was used to expand starch-based compositions. Foam beads made by solvent extraction had the appearance of polystyrene beads but did not expand when heated due to an open-cell structure. Nonporous beads, pellets, or particles were made by extrusion or by drying and milling cooked starch slurries. The samples expanded into a low-density foam by heating 190-210 degrees C for more than 20 s at ambient pressures. Formulations containing starch (50-85%), sorbitol (5-15%), glycerol (4-12%), ethylene vinyl alcohol (EVAL, 5-15%), and water (10-20%) were studied. The bulk density was negatively correlated to sorbitol, glycerol, and water content. Increasing the EVAL content increased the bulk density, especially at concentrations higher than 15%. Poly(vinyl alcohol) (PVAL) increased the bulk density more than EVAL. The bulk density was lowest in samples made of wheat and potato starch as compared to corn starch. The expansion temperature for the starch pellets decreased more than 20 degrees C as the moisture content was increased from 10 to 25%. The addition of EVAL in the formulations decreased the equilibrium moisture content of the foam and reduced the water absorption during a 1 h soaking period.  相似文献   

16.
Sorghum (Sorghum bicolor (L.) Moench) grain was boiled or autoclaved in alkali, washed, drained, and dried into shelf-stable half-products (pellets). The pellets were deep-fat fried to produce a crunchy snack product. Effects of cooking time, drying method (pellet moisture content), and sorghum cultivar on unfried and fried pellets were evaluated. Increasing the alkaline cooking time from 30 to 60 min decreased the yield of the pellets from 96 to 84% (on a dry weight basis). Cooked sorghum dried at room temperature (24°C) for 18 hr, followed by oven-drying at 50°C for an additional 18 hr, produced pellets with a low moisture content (≤5%), that required a higher frying temperature (≥220°C). However, cooked sorghum dried at room temperature for 18 hr followed by oven-drying at 50°C for 5 hr produced pellets with 9% moisture and a lighterdensity highly acceptable product when fried at 220°C. Fat content of fried pellets averaged 18%. The optimum method for producing a light, crunchy, fried product was cooking for 60 min, drying to 9% moisture, and frying at 220°C. ATx631*Tx436, the hardest endosperm-texture sorghum used in the study, had the highest unfried and fried pellet yields. Dorado, an intermediate-to-soft endosperm-texture sorghum, and ATx Arg-1*Tx2907, a waxy sorghum, had lower yields. The fried pellets produced from Dorado and waxy sorghum (ATxArg-1*Tx2907) were more expanded than those produced from ATx631*Tx436.  相似文献   

17.
The effect of hydrocolloids addition (0, 25, or 1.5 g/100 g of flour) on water absorption of flour and their influence on dough rheology were analyzed. The influence of guar gum (GG), xanthan gum (XG), high‐methoxyl pectin (P), locust bean gum (LBG), and a 1:1 mixture of locust bean gum and xanthan gum (LBG+XG) on water absorption was tested by different techniques including farinograph water absorption, water imbibing capacity, SDS sedimentation test, and sucrose solvent retention capacity. The rheological behavior was analyzed through the farinograph parameters and texture profile analysis (TPA). Principal component analysis (PCA) was applied to evaluate the behavior of the different mixtures. Absorption values obtained by different methods were increased by XG and LBG+XG addition, particularly at the highest levels (1–1.5%). Flour‐P mixtures showed the lowest absorption. GG‐added mixtures led to the more stable doughs and P to the less stable ones. Addition of NaCl increased stability in all cases. According to TPA, softer and less cohesive doughs than control were obtained when hydrocolloids were added, both in conditions of water availability and water restriction (except for XG and GG at the highest levels). However, when enough water was added, more variation in textural attributes among doughs could be observed by PCA. No remarkable differences compared with the control were observed in the gluten network, as evaluated by scanning electron microscopy. Hydrocolloid incorporation led to rheological changes in dough; the trend and degree of this effect was affected by the amount of water added and the structure and concentration of the hydrocolloid.  相似文献   

18.
Guar gum, a nonionic galactomannan, is used as an economical thickener and stabilizer in the food industry and is often combined with xanthan, locust bean gum (LBG), or carboxymethylcellulose (CMC) to promote synergistic changes in viscosity or gelling behavior via intermolecular interactions; however, the adulteration of LBG with guar gum is a well-known industrial problem. The ability to identify the purity of gums and concentrations of individual gums in mixtures would be advantageous for quality control in the food industry. Fourier transform infrared spectroscopy (FTIR) methods are rapid and require minimum sample preparation. The objectives of this study were to evaluate the ability of FTIR techniques to (1) differentiate LBG with a variety of mannose/galactose (M/G) ratios, (2) differentiate guar, LBG, tara, and fenugreek gums, (3) differentiate pure guar gum from guar gum mixed with LBG, xanthan gum, or CMC, (4) quantify LBG, xanthan gum, and CMC in guar gum, and (5) quantify guar gum in LBG. Two FTIR methods were used: diffuse reflectance (DRIFT) on powdered gum samples added to KBr at 5%, w/w, and attenuated total reflectance (ATR) on 1%, w/w, gum solutions. Spectra were collected and then analyzed by multivariate statistical procedures (chemometrics). The DRIFT method provided better discrimination and quantitative results than the ATR method. Canonical variate analysis (CVA) of DRIFT spectra (1200-700 cm(-1)) was able to classify LBG with various M/G ratios, pure galactomannans, and pure versus mixtures of gums with 100% accuracy. Quantification of an individual gum in gum mixtures (0.5-15%, w/w) was possible using partial least-squares (PLS) analysis of DRIFT spectra with R2 > 0.93 and using this approach for quantifying guar gum added to LBG resulted in an R2 > 0.99, RMSEC = 0.29, and RMSEP = 3.31. Therefore, the DRIFT FTIR method could be a useful analytical tool for quality control of select gums and gum mixtures used in the food industry.  相似文献   

19.
微波干燥过程中南极磷虾肉糜的传热传质及形变参数模型   总被引:6,自引:6,他引:0  
该文以南极磷虾肉糜作为媒介,基于电磁学、多相传输和固体力学变形模型研究了微波干燥仿真模型。通过在软件COMSOL Multiphysics中求解电磁方程、能量和动量守恒以及变形方程得到模拟结果。红外热成像仪用于拍摄样品表面温度分布,光纤传感器用于测定样品点的瞬时温度。经过180 s的间歇微波干燥,空间温度分布、瞬态温度曲线(RMSE=2.11℃)、含水率(干基,RMSE=0.03)和体积比与试验值有良好的一致性,说明仿真微波干燥是可行的。此外,微波模拟干燥过程中将虾肉糜视为形变材料与刚性材料,在温度和含水率方面显示了较明显的差别且前者与试验值更为接近,且未考虑收缩模型的温度和含水率的RMSE分别为9.42℃与0.08。该研究还对液态水和气体的内在渗透性(±50%)以及吸水膨胀系数(±50%)进行了敏感性分析。含水率对液态水的内在渗透性较敏感(RMSE=0.089),对气体的内在渗透性较不敏感(RMSE=0.023),体积比对吸水膨胀系数非常敏感(RMSE=0.053)。  相似文献   

20.
Rice pellets were prepared by single‐screw extrusion cooking with an in‐barrel water content of 50 wt%. Three different types of rice, indica glutinous, japonica, and indica, were used as raw materials. Reconstituted rice flour was made to study the effect of amylose content on pellet expansion. The glass transition (Tg) and expansion (Te) temperatures of extruded pellet were determined by differential scanning calorimetry (DSC) and noncontact infrared thermometer, respectively. The amylose content was not significantly affected by extrusion cooking. The reduction in intrinsic viscosity indicated that amylopectin experienced some degradation. The Tg and Te were not functions of amylose content, which affected the expansion ratio of the pellets. The Gordon‐Taylor equation was applied to estimate the Tg of the rice pellets.  相似文献   

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