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1.
Twenty-four Spanish thyme honey samples were analyzed using inductively coupled plasma optical emission spectrometry (ICP-OES). Twenty-four minerals were quantified for each honey. The elements Al, As, Ba, Ca, Cr, Cu, Fe, K, Li, Mg, Mn, Na, P, Pb, S, Se, Si, Sr, and Zn were detected in all samples; seven elements are very abundant (Ca, K, Mg, Na, P, S, and Si), and six are not abundant (Al, Cu, Fe, Li, Mn, and Zn). Eleven of them are trace elements (As, Ba, Cd, Co, Cr, Ni, Mo, Pb, Se, Sr, and V) at <1 mg kg(-)(1). Classification of thyme honeys according to their origin (coast, mountains) was achieved by pattern recognition techniques on the mineral data. By means of principal component analysis, a good separation by geographical origin is obtained when scores for the two first principal components are plotted. Classification functions of 11 metals (Al, As, Cr, Cu, K, Li, Mg, Na, P, S, and V) were obtained using stepwise discriminant analysis and applied to classify correctly approximately 100% of the honey samples. 相似文献
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中国烤烟中部叶矿质营养元素浓度状况 总被引：13，自引：1，他引：13
于20012～004年,从重点植烟县采集了410个烤烟中部叶样品,运用ICP测定方法和概率密度分布函数对其氮、钾、磷、钙、镁、硫、锰、铜、锌、硼、钠、铁、氯13个矿质元素的浓度特征进行了分析。结果表明:1)大量元素的变异系数较小,中量元素其次,微量元素较大;2)除氮、镁、硫、铜、锌、钠、铁外,其他元素的浓度在品种之间的差异显著,但不同指标在品种之间的高低秩序不同,例如,云烟87的磷浓度显著地高于云烟85、K326的磷浓度,而钾浓度按K326、云烟87、云烟85依次降低;3)所有元素在省份之间的差异极显著,但不同元素在地区之间的高低秩序不同,例如,河南烟叶的钾浓度显著地低于其他省份,贵州烟叶的氯离子浓度显著地高于其他地方;4)钾、磷、钙、硫、硼、钠在烟叶中的浓度符合正态分布,氮、镁、氯、锰、铜、锌、铁在烟叶中的浓度符合对数正态分布;5)氮、磷、钾、钙、镁、硫、锰、铜、锌、硼、钠、铁、氯的正常浓度范围分别为1.18～2.34、0.11～0.30、0.87～2.83、0.99～3.64、0.1～0.8、0.25～0.9、25.18～601.65、2.1～37.271、3.11～105.421、2.6～55.62、163.02～503.11、97.6～384.2、0.07～0.53(氮、磷、钾、钙、镁、硫、氯的单位为%,其余为mg/kg);6)氮、钾、氯、钾/氯比四个因素符合国际型优质烟叶质量标准的概率只有0.726、0.379、0.193、0.829,目前我国烤烟营养不够协调的主要方面是养分浓度偏低。 相似文献
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4.
《Communications in Soil Science and Plant Analysis》2012,43(7-8):803-825
Abstract Apple seedlings from a greenhouse pot experiment, investigating the effects of copper (Cu) and peat amendments on crop performance growing on a Cu‐and potassium (K)‐deficient soil, were characterized for a range of major and trace elements. Concentrations of barium (Ba), calcium (Ca), Cu, iron (Fe), K, magnesium (Mg), manganese (Mn), molybdenum (Mo), sodium (Na), rubidium (Rb), strontium (Sr), and zinc (Zn) in leaf and stem tissues were correlated with treatment and tissue. Addition of Cu, peat and the nature of the tissue had significant impacts on many element concentrations. Generally, increasing Cu resulted in elevated Ba, Fe, Mo, and Sr as well as Cu levels. The presence of peat resulted in reduced levels, generally in both leaf and stem, of Ba, Mg, Mn, Rb, and Zn and increased levels of Fe, K, and Mo. Finally, the vast majority of elemental concentrations were higher in leaf tissue rather than stem, with the exceptions of Na and Zn. Elemental concentration ranges, over all tissues and conditions of added Cu and peat were (mg kg‐1) Ba 9–49, Ca 6380–16340, Cu 2–11, Fe 10–57, K 4070–16950, Mg 900–4260, Mn 22–197, Mo 0.02–0.19, Na 28–124, Rb 0.7–12, Sr 41–58, Zn 18–48. 相似文献
5.
营养液供液高度对水培生菜生长及矿质元素吸收的影响 总被引：1，自引：0，他引：1
在密闭植物工厂条件内,设置5种营养液高度（2、3、4、5、6cm）水培种植生菜,以探究霍格兰（Hoagland）配方营养液不同供液高度对生菜十种矿质元素（K、P、Ca、Mg、Na、Fe、Mn、Zn、Cu、S）吸收及积累的影响。结果表明：生菜地上部生物量以及光合色素含量均在4cm供液高度处理下最大,而地下部生物量以及根长均随着营养液供液高度的增加而升高;生菜地上部十种矿质元素的含量均在供液高度6cm处理下最大,而矿质元素在生菜中的单株累积量则表现为Fe、Mn元素在6cm供液高度下最大,Ca、Mg、Na、Zn、Cu、S元素在4cm供液高度下最大,K、P元素在5cm供液高度下最大。因此,实际生产中可以通过调节水培生菜营养液的供液高度,以达到提高生菜产量或生产功能性蔬菜的目的。 相似文献
6.
Kyle Devey Michael Mucalo Gordon Rajendram Joseph Lane 《Communications in Soil Science and Plant Analysis》2015,46(4):72-80
Laser-induced breakdown spectroscopy (LIBS) is a new technique for the analysis of plant material. This study investigates the application of LIBS to pasture-based plant samples. The LIBS measurements were obtained from pelletized pasture samples (100 samples) that had been also analyzed by inductively coupled plasma–optical emission spectroscopy (ICP-OES) following microwave digestion for calibration and comparison purposes. Comparisons for elements sodium (Na), potassium (K), magnesium (Mg), calcium (Ca), manganese (Mn), iron (Fe), copper (Cu), zinc (Zn), boron (B), phosphorus (P), and sulfur (S) showed that LIBS could be used for almost all the standard profile total elements with concentrations down to low mg/kg levels (observed error of Na: 0.024 percent, K: 0.18 percent, Mg: 0.016 percent, Ca: 0.073 percent, P: 0.017 percent, Mn: 31 mg/kg, Fe: 150 mg/kg, Zn: 6.6 mg/kg, and B: 1.1 mg/kg). Elemental analysis at less than mg/kg levels was not possible using LIBS. The elements S and Cu were particularly difficult to analyze with reliability using LIBS at the concentration levels found in the plant samples. Replacing microwave digestion and subsequent ICP analysis with a direct analysis of dried plant samples using LIBS has the potential to improve the productivity and reduce the cost of testing. 相似文献
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The dry weight accumulation per male and female flower as well as the concentration per gram of dry weight and the accumulation of nitrogen (N), phosphorus (P), potassium (K), calcium (Ca), magnesium (Mg), iron (Fe), manganese (Mn), zinc (Zn), and copper (Cu) were determined in walnut tree (Juglans regia L.) catkins and female flowers at the stage of flower bud and during the flower development. Catkin emergence was accompanied by a very fast hydration of the tissues. After the catkin matured, the fresh and dry weights were reduced. The female flower development period was accompanied by the dry and fresh weight increase. Total N, P, K, Fe, Mn, Cu and Zn concentrations in catkin buds were detected at lower levels, Mg in equal levels, and Ca at higher levels as compared to the nutrient concentrations in young growing leaves. The estimated values of the ratio NCmfb/NCygl were: total N = 0.54, P = 0.83, K = 0.56, Ca = 1.5, Mg = 1.0, Fe = 0.46, Mn = 0.71, Cu = 0.85, and Zn = 0.60. Nutrient concentration in female flower buds was detected in almost equal levels with the exception of total N and Fe. The estimated values of the ratio: NCffb/NCygl were: total N = 0.57, P = 1.1, K = 1.17, Ca = 1.06, Mg = 0.9, Fe = 0.47, Mn = 1.0, Cu = 0.92, and Zn = 0.85. Total N, P, Mn, Cu, and Zn accumulations in the catkin were increased during the fast growing phase and decreased after catkin maturing. Potassium, Mg, and Fe accumulation continued to increase in the mature catkin. Calcium accumulation decreased at a very late mature catkin phase. Total N, P, and K accumulation rates during the catkin fast growing phase were higher than the dry weight accumulation rate. Calcium, Mg, Fe, Mn, Cu, and Zn accumulation rates at the same period were lower or equal to dry weight accumulation rates. In mature catkins, the total N, P, Mn, Cu, and Zn depletion rates were higher than the dry weight depletion rate. The continual increase of K, Ca, Mg, and Fe accumulation in mature catkin resulted in the increase of nutrients concentration also. Total N and P showed the highest remobilization values from mature catkin of 51.4% and 45%, respectively. Calcium, K, Mg, Cu, Mn, and Zn remobilization values estimated to be 22.1%, 7.5%, 3.2%, 45.3%, 33.4%, and 31.8%, respectively. Iron showed no remobilization at all. Nutrients remobilization from catkins as compared to the leaves had almost similar values for total N, Zn, and Cu, higher for P, Ca, and Mn, and lower for Mg, Fe, and K. Accumulation of all nutrients in female flowers increased after fertilization. The dry weight accumulation rate was higher than the nutrient accumulation rates. 相似文献
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《Communications in Soil Science and Plant Analysis》2012,43(11):969-979
Abstract Insoluble siliceous residues remaining after HNO3/HClO4 decomposition of the plant tissues National Bureau of Standards, standard reference materials spinach (Spinacea oleracea), orchard leaves and tomato leaves (Lycopersicon escuientum), contained varying quantities of the macro and micro elements Na, K, Mg, Ca, Mn, Fe, Cu and Zn. For the different samples with total element concentrations ranging from 11 μg/g (Cu in orchard leaves) to 45,000 μg/g (K in tomato leaves), residues contained element concentrations ranging from 0.05 to 88 times the respective concentrations in the samples. Contributions of residues to element concentrations in the plant tissues varied from 0.04 to 42% of the total concentrations. Overall, these constituted negligible (ca 0.1% for Mg and Ca), small (0.5% for Zn, Mn, K and 1% for Cu), and large (6% for Fe, 28% for Na) contributions depending on sample and analyte. Residue contributions to total element concentrations of plant tissues must be considered for reliable estimations of macro and micro elements. 相似文献
9.
The concentration of major and trace elements was determined for tomato (Lycopersicon esculentumcv. Aromata F1) fruits grown in three different substrate systems. The systems were soil and rockwool irrigated with a normal nutrient solution and rockwool irrigated with a nutrient solution with elevated electrical conductivity (EC). At three harvest times, tomato fruits were analyzed for Ca, Cu, Fe, K, Mg, Mn, Na, P, S, Sr, and Zn by ICP-AES and for Cd, Cr, Mo, Ni, Pb, Sn, and V by HR-ICPMS. The concentrations of Ca, Cd, Fe, Mn, Mo, Na, Ni, Sr, and Zn were significantly different (p < 0.05) for tomato fruits grown on the different substrates. Between the harvest times different levels (p < 0.05) were shown for Ca, Cd, Fe, Mn Na, Ni, Sr, Zn Cu, K, Mg, P, Sn, and V. The concentration of Cd was >15 times higher and the concentration of Ca was 50-115% higher in soil-grown fruits than in rockwool-grown fruits. Principal component analysis applied on each harvest split the data into two groups. One group includes soil-grown fruits, and the other group includes rockwool-grown fruits with the two different nutrient solutions. 相似文献
10.
Ali A. Al‐Jaloud Ghulam Hussain Adnan J. Al‐Saati Shaik Karimulla 《Journal of plant nutrition》2013,36(8):1677-1692
Effect of wastewater irrigation was investigated on mineral composition of corn and sorghum plants in a pot experiment. The ranges for the concentration of different minerals in corn plants were 0.67–0.89% calcium (Ca), 0.38–0.58% magnesium (Mg), 0.09–1.29% sodium (Na), 0.81–1.87% nitrogen (N), 1.81–2.27% potassium (K), 0.12–0.16% phosphorus (P), 190–257 mg/kg iron (Fe), 3.5–5.6 mg/kg copper (Cu), 37.1–44.5 mg/kg manganese (Mn), 21.6–33.6 mg/kg zinc (Zn), 1.40–1.84 mg/kg molydbenum (Mo), 11.0–45.7 mg/kg lead (Pb), and 2.5–10.8 mg/kg nickel (Ni). Whereas for sorghum plants, the ranges were: 0.56–0.68% Ca, 0.19–0.32% Mg, 0.02–0.27% Na, 0.69–1.53% N, 1.40–1.89% K, 0.10–0.14% P, 190–320 mg/kg Fe, 3.8–6.0 mg/kg Cu, 29.2–37.6 mg/kg Mn, 21.1–29.9 mg/kg Zn, 2.2–3.7 mg/kg Mo, 12.3–59.0 mg/kg Pb, and 2.5–15.2 mg/kg Ni. Heavy metals such as cobalt (Co) and cadmium (Cd) were below detection limits at mg/kg levels. The concentrations of Ca, N, K, P, Cu, and Mn in corn plants were in the deficient range except for Mg, Fe, Zn, and Al. The concentrations of Ca, N, P, K, Cu, Mn, Mg, and Zn in sorghum plants were in the deficient range except for Fe and aluminum (Al). The analysis of regression indicated a strong interaction between Pb, Ni, Ca, and Fe in corn and sorghum plants. In conclusion, waste water irrigation did not increase mineral concentrations of either macro‐ and micro‐elements or heavy trace metals in corn and sorghum plants to hazardous limits according to the established standards and could be used safely for crop irrigation. 相似文献
11.
《Communications in Soil Science and Plant Analysis》2012,43(5-6):569-583
Abstract X‐ray fluorescence (XRF) is an effective and rapid technique for the analysis of many mineral elements in plant tissue. Plant samples sometimes are too small to make good pellets and to provide good XRF analyses. Leaf tissue was mixed with cellulose or boric acid at different ratios to assess whether pellets from these mixtures could be analyzed by XRF and to determine the effects of these inert substances on analysis of Al, Ca, Cl, Cu, Fe, K, Mg, Mn, P, S, Si, and Zn. Concentrations of all elements decreased linearly at all leaf/cellulose ratios. Concentrations of Mn, Fe, Zn, and Cu decreased linearly at all leaf/boric acid ratios, but concentrations of the other elements decreased linearly only when leaf/boric acid ratios were above about 40/60, and decreases in concentration of these other elements were more pronouned at leaf/boric acid ratios below 40/60. Concentrations of P, S, Cl, K, Mg, Ca, Si, and Al were higher in leaf/boric acid than in leaf/cellulose pellets, and similar concentrations were noted for Cu, Mn, Fe, and Zn in both kinds of pellets. Mechanically shaking cellulose with leaf tissue generally resulted in higher mineral element concentrations than if samples were mixed by hand. Cellulose would be the preferred inert substance to mix with plant samples if plant samples are below ～40 mg in size. Small samples of plant tissue can effectively be analyzed by XRF when mixed with cellulose or boric acid. 相似文献
12.
《Communications in Soil Science and Plant Analysis》2012,43(9-10):1383-1396
Abstract Near infrared reflectance spectroscopy (NIRS) was tested to predict the nitrogen (N) and mineral concentration [for the elements phosphorus (P), potassium (K), calcium (Ca), magnesium (Mg), sodium (Na), manganese (Mn), iron (Fe), copper (Cu), and zinc (Zn)] in natural grassland samples. The samples wrere taken from different community types according to the topographic gradient at different maturation stages and during a period of four consecutive years. A subset of 95 samples was selected on the basis of the spectral variation. Chemical values from the calibration sample set were regressed on the corresponding spectral data using a stepwise multiple regression analysis. Another subset of 75 samples was used as the validation set. Standard errors of prediction and correlation coefficients, respectively, were: 0.71 and 0.97 (N), 0.22 and 0.73 (P), 1.83 and 0.84 (K), 0.83 and 0.92 (Ca), 0.15 and 0.92 (Mg), 3.94 and 0.66 (Na), 44 and 0.84 (Mn), 19 and 0.75 (Fe), 1.01 and 0.77 (Co), and 3.9 and 0.79 (Zn). 相似文献
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重庆缙云山酸沉降背景下针阔混交林水化学特征初步研究 总被引：1，自引：0，他引：1
选取三峡库区缙云山小流域针阔混交林作为研究对象,对其大气降水、穿透雨、树干茎流、地表径流等水文过程中的pH值及Na+、K+、Ca2+、Mg2+等离子含量进行研究,结果表明:(1)大气降水pH值为5.31,呈酸性,已属于酸雨范围(pH<5.65)。相对于大气降水,针阔混交林穿透雨和树干茎流离子含量均大幅增加。穿透雨和树干茎流中,Mg、Cu元素的变异系数均小于大气降水,而K、Zn和Mn均大于大气降水。地表径流中Ca元素含量最高,为16.416mg/L,Mn元素含量最低,几乎检测不到。各元素含量排序为:Ca>K>Na>Mg>Zn>Fe>Cu>Mn。地下径流中,Ca元素是含量增加最多的养分元素,各元素含量排序为:Ca>K>Na>Mg>Zn>Cu>Fe=Mn。(2)Cu元素在穿透雨和树干茎流中均出现了负淋溶,其余各元素浓度均有所增加。如果林木长期处于酸雨逆境下,将会导致部分营养元素大量流失,并最终造成林木营养亏损且影响其生长。 相似文献
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Gonzálvez A Armenta S Pastor A de la Guardia M 《Journal of agricultural and food chemistry》2008,56(13):4943-4954
Different sample preparation methods were evaluated for the simultaneous multielement analysis of wine samples by inductively coupled plasma optical emission spectrometry (ICP-OES) and inductively coupled plasma mass spectrometry (ICP-MS). Microwave-assisted digestion in closed vessel, thermal digestion in open reactor, and direct sample dilution were considered for the determination of Li, Be, Na, Mg, Al, K, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Sr, Y, Mo, Cd, Ba, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Tl, Pb, and Bi in 12 samples of red wine from Valencia and Utiel-Requena protected designation of origin. ICP-MS allows the determination of 17 elements in most of the samples, and using ICP-OES, a maximum of 15 elements were determined. On comparing the sample pretreatment methodology, it can be concluded that the three assayed procedures provide comparable results for the concentration of Li, Na, Mg, Al, K, Ca, Mn, Fe, Zn, and Sr by ICP-OES. Furthermore, ICP-MS data found for Cu, Pb, and Ba were comparable. Digestion treatment provides comparable values using both total decomposition in open system and microwave-assisted treatment for Cu by ICP-OES and for Cr, Ni, and Zn by ICP-MS. Open vessel total digestion provides excess values for Cr, Mn, Fe, and Zn by ICP-OES and defect values for Se. However, direct measurement of diluted wine samples provided uncomparable results with the digestion treatment for Mn, Cu, Pb, Zn, Ba, and Bi by ICP-OES and for Mg, Cr, Fe, Ni, and Zn by ICP-MS. Therefore, it can be concluded that microwave-assisted digestion is the pretreatment procedure of choice for elemental analysis of wine by ICP-based techniques. 相似文献
15.
《Communications in Soil Science and Plant Analysis》2012,43(6):895-902
Abstract Seasonal changes in leaf element composition were measured at 2‐week intervals in A Oregon cranberry bogs from June 1 to September 15 for a 3‐year period. Nitrogen, P, K, and Zn leaf concentrations decreased during the season while concentrations of Ca, Mg, B, Mn, and Fe increased. Periods of 30‐day minimal internal flux varied from July 15 to September 15, depending on the element. It was concluded that 2 samples, 1 from June 15 to July 15 for Mg, Mn, and Fe and 1 from August 15 to Sep‐ tember 1 for N, P, K, Ca, Cu, B, and Zn, would have to be taken to adequately diagnose the nutrient status of all of the essential elements for cranberry. 相似文献
16.
Kwoczek M Szefer P Hać E Grembecka M 《Journal of agricultural and food chemistry》2006,54(8):3015-3024
The concentrations of 15 elements (Cu, Fe, Mn, Zn, Co, Ni, Cr, Se, Cd, Pb, Hg, Ca, Na, K, and Mg) were determined in the edible parts of shellfish on sale in the local market in Gdańsk. The samples consisted of three groups--crustaceans, molluscs, and surimi--that are processed to different degrees. For the purposes of this analysis, they were dried, homogenized, and digested in an automatic microwave system. The samples were analyzed quantitatively for Cu, Zn, Fe, Mn, Co, Ni, Cr, Mg, Na, K, and Ca (F-AAS), Cd and Pb (GF-AAS), Se (HG-AAS), and Hg (CV-AAS). The elemental levels detected in shellfish were compared to those in cod, herring, pork, beef, chicken, and eggs. The recommended dietary allowance (RDA) of essential elements and the provisional tolerable weekly intake (PTWI) of toxic elements were estimated. With factor analysis of the data, taxonomically different groups of raw and processed shellfish could be distinguished. 相似文献
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为了解在成龄胶园间作的五指毛桃根际与非根际土壤及其根中主要中、微量元素含量情况，测定了实验区根际与非根际土壤各30个和对应五指毛桃根的钙、镁、铁、锰、铜和锌含量，分析了两者之间的关系，并评价了根际与非根际土壤中、微量元素丰缺状况。结果表明，非根际土壤钙、镁、铁、锰含量的平均值都高于根际土壤的，而铜、锌含量的平均值都低于根际土壤的。土壤钙、镁含量80%以上处于缺水平，而铁、锰含量处于丰或很丰水平，铜和锌含量处于适中水平。五指毛桃根际与非根际土壤中、微量元素存在空间上的广泛变异。五指毛桃根中、微量元素的平均值从大到小的排序是钙>镁>锰>铁>锌>铜。土壤中、微量元素与五指毛桃根中相对应的中、微量元素的相关性不强，且表现复杂。本研究结果揭示，在成龄胶园间作五指毛桃应当适量施用钙肥、镁肥和喷施一些铜元素叶面肥，并实行科学施肥，减少养分淋失。 相似文献
19.
《Communications in Soil Science and Plant Analysis》2012,43(1-2):82-95
Abstract A compost of high copper (Cu) and zinc (Zn) content was added to soil, and the growth of barley (Hordeum vulgare L.) was evaluated. Four treatments were established, based on the addition of increasing quantities of compost (0, 2, 5, and 10% w/w). Germination, plant growth, biomass production, and element [nitrogen (N), phosphorus (P), potassium (K), calcium (Ca), sodium (Na), magnesium (Mg), iron (Fe), Cu, manganese (Mn), and Zn] contents of soil and barley were determined following a 16‐week growing period. Following harvesting of the barley, analysis of the different mixtures of soil and compost was performed. Micronutrient contents in soils as affected by compost additions were determined with diethylene–triamine–pentaacetic acid (DTPA) (Cu, Mn, Fe, and Zn) or ammonium acetate [Ca, Na, Mg, K, cation exchange capacity (CEC)] extractions, and soils levels were compared to plant uptake where appropriate. Increasing rates of compost had no affect on Ca, Mg, or K concentration in barley. Levels of Cu, Zn, Mn, and Na, however, increased with compost application. High correlations were found for DTPA‐extractable Cu and Zn with barley head and shoot content and for Mn‐DTPA and shoot Mn content. Ammonium acetate–extractable Na was highly correlated with Na content in the shoot. High levels of electrical conductivity (EC), Cu, Zn, and Na may limit utilization of the compost. 相似文献
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《Communications in Soil Science and Plant Analysis》2012,43(17):2524-2534
Lack of microelements is a major problem in crop production in tropical peatland. For their efficient application, the fate of copper (Cu), iron (Fe), manganese (Mn), and zinc (Zn) in a Histosol was investigated in a 3-month column experiment. Leaching of Cu, Fe, Mn, and Zn accounted for 2, –2 to 7, 28 to 32, and 21 to 23% of the amounts applied, respectively, in both the flooded and upland soils. The microelement application enhanced the leaching of calcium (Ca), potassium (K), magnesium (Mg), sodium (Na), and phosphorus (P). Replacement of exchangeable cations by the microelements was suggested in the successive extraction of elements from the soils after incubation. Under the upland conditions, 31–33% of the Cu and Fe increased in soil was extracted with diethylenetriaminepentaacetic acid?/?triethanolamine (bound to humus), whereas 26–31% of the Mn and Zn increased was exchangeable. Extractability was smaller under the flooded conditions for all the microelements, suggesting that fertilization in the dry season is more effective. 相似文献