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1.
苦楝素提取方法的比较研究   总被引:11,自引:1,他引:10  
对比研究了从苦楝树皮中提取苦楝素的几种方法,通过实验,得出了不同提取方法的最佳条件。超临界CO2萃取在萃取温度45℃、压力20MPa、夹带剂为60%乙醇的情况下萃取2h,苦楝素的萃取率为0.850%;微波辅助提取法,以60%乙醇为溶剂,料液比为1∶9(g∶mL,下同),微波功率340W,辐射时间40s×3次,苦楝素的提取率为0.693%;超声波提取法,以60%乙醇为溶剂,料液比为1∶9,超声波作用时间为30min,超声波功率为200W,苦楝素的提取率为0.715%。将上述3种提取方法与传统的有机溶剂提取法进行详细的比较,结果表明:对于苦楝素提取,超声波提取法最好。  相似文献   

2.
正交试验法优选沙棘总黄酮的超声波提取工艺   总被引:10,自引:0,他引:10  
以沙棘叶为原料,用正交试验法优化了沙棘总黄酮(TFH)的超声波提取工艺,考察了超声波作用时间、超声波温度、液料比和提取次数4个因素对沙棘总黄酮提取率的影响,确立了沙棘总黄酮的优化超声波提取工艺条件为:提取溶剂85 %乙醇,液料比25∶1(mL∶g,下同),超声波温度46 ℃,超声波作用时间25 min,提取1次.将该法与索氏提取进行了对比.结果表明,超声波提取沙棘总黄酮的提取率为1.72 %,与索氏提取的提取率相当,但超声波提取所用提取时间短,提取溶剂用量少,因此超声波法具有明显的优势.同时对超声波提取进行了数学模拟,模拟值与试验结果吻合良好.  相似文献   

3.
超声波提取杜仲皮总黄酮工艺   总被引:1,自引:0,他引:1  
以杜仲皮为原料,采用单因素和正交试验,探讨了超声波提取杜仲皮内黄酮的最佳工艺条件。结果表明:采用体积分数95%的乙醇为提取液,杜仲皮与提取液的料液比为1∶40(g∶mL),每次超声波处理时间为30 min,超声波功率50 W为最佳提取条件,在该条件下黄酮提取率为10.01%。  相似文献   

4.
采用超声波辅助提取法,对淡竹叶总黄酮和固形物得率的工艺条件进行研究。以水为提取溶剂,通过单因素试验研究提取温度、提取时间、超声功率、料液比以及提取次数等对淡竹叶黄酮得率和固形物得率的影响。在单因素的基础上,通过正交试验对超声波辅助提取淡竹叶黄酮和固形物的工艺进行优化。结果表明:超声波辅助提取淡竹叶总黄酮的最佳工艺条件为提取时间40 min,料液比1∶20,超声温度70℃,超声频率40 k Hz。在此最佳工艺条件下总黄酮得率为1.23%。超声波辅助提取固形物的最佳工艺条件为提取时间50 min,料液比1∶40,超声温度70℃,超声频率50 k Hz。在此最佳工艺条件下固形物得率为13.15%。  相似文献   

5.
蚬壳花椒总生物碱的提取工艺   总被引:3,自引:0,他引:3  
采用回流提取法,通过单因素试验和正交试验,研究了蚬壳花椒茎中总生物碱的提取工艺,用干重法及酸性染料比色法测定总生物碱含量.结果表明,最佳提取溶剂为乙醇,总生物碱最佳提取条件为:超声波提取1 h,浸泡48 h后,75%体积分数的乙醇为溶剂,料液比为1:25,pH值为2.0,70 C回流提取2 h,蚬壳花椒茎的总生物碱的提取率达5.57%.  相似文献   

6.
正交设计提取梨皮总黄酮   总被引:8,自引:0,他引:8  
用正交试验法对梨皮中的黄酮类化合物提取工艺进行了优选研究。采用正交表L1 6(4 5 ) ,以提取时间、提取温度、提取次数、提取剂中乙醇含量以及料液比为因素 ,以总黄酮显色液的吸光度为指标进行试验。得到了最佳提取参数 :温度为 70℃ ,时间 2h ,提取次数 3次 ,提取溶剂为 80 %的乙醇 ,料液比为 1∶7。  相似文献   

7.
采用超声辅助提取法从无患子果皮中提取无患子皂苷,通过单因素试验考察了乙醇浓度、提取时间、料液比以及提取次数4个因素对无患子皂苷得率的影响,并采用响应面法确定无患子皂苷的最佳提取工艺条件为:乙醇体积分数82.2%、提取时间33.75 min、料液比1:28.9、提取次数4次,在此优化条件下无患子皂苷的理论提取率可达到21.52%。依实际试验情况,将其修正为乙醇体积分数82%、提取时间34 min、料液比1:29、提取次数4次,经验证此条件下无患子皂苷提取率为21.48%,与理论值较为接近,表明采用响应面法分析优化无患子皂苷超声辅助提取工艺的方法可行。  相似文献   

8.
以自制白果粉为原料,分析了提取溶剂、粉料粒度、提取温度、超声波功率、料液比、提取时间及提取次数对白果出油率的影响。结果表明:石油醚(沸程60~90℃)是较适宜的提取溶剂,出油率为3.88%。最佳提取工艺为:白果粉粉碎度80目,提取温度25℃,超声波提取功率200 W,料液比1∶25(g/ml),每次提取时间40 min,提取次数2次。最优工艺条件下,出油率为3.86%,较索氏提取法,该工艺对白果粗脂肪的提取率为98.71%。  相似文献   

9.
以鲜姜黄为原料,对姜黄素的匀浆提取进行了研究,确定采用75%乙醇为溶剂,匀浆3 min,转速8 000 r/min,料液比为1∶9(g/mL)为最佳提取条件。姜黄素的提取率可达63.45%。相对回流提取法,匀浆提取具有操作简便,提取率高的优点。  相似文献   

10.
金银花中总黄酮的超声波提取工艺优化   总被引:1,自引:0,他引:1  
黄小梅  邓祥  吴狄  王坤 《绿色科技》2013,(11):14-16,19
采用超声波法提取了金银花中的总黄酮,通过单因素试验研究了乙醇体积分数、超声温度、超声时间、料液比和超声频率等因素对提取效率的影响。在此基础上,选择乙醇体积分数、超声温度、料液比和超声时间进行L9(34)正交试验,得出了总黄酮的最佳提取工艺参数:乙醇体积分数为70%,超声温度为50℃,料液比为1∶25(g · mL1),超声时间为2.0h ,超声功率为900W ,最大提取率达到9.37%。  相似文献   

11.

In Scandinavia, moose (Alces alces L.) sometimes cause severe browsing damage to economically-important pine. Moose-vehicle accidents have spurred construction of fences along roads, and these may interfere with moose migration between summer and winter ranges, or the road alone may be a barrier. If this happens and moose build up along roads, landowners may suffer economically. Therefore, this study investigated whether roads, fences or other factors influence the use of young pine stands by moose. Eighty stands along roads in northern Sweden were evaluated in which individually-browsed branches were counted on 9972 pines. Moose browsing was not significantly related to birch (Betula pendula Roth, B. pubescens Ehrh.) density, nor did it differ between pines (Pinus contorta Douglas or P. sylvestris L.). However, increased pine density, site productivity and proximity to a highway were associated with increased browsing. Further large-scale studies are needed to understand moose habitat selection and the effects of roads.  相似文献   

12.

The root systems of 2-yr-old Picea glauca, Picea mariana and Pinus banksiana seedlings were submitted to various frost temperatures during an artificial frost to induce different levels of root damage. Frost-damaged and control seedlings were placed in a greenhouse under high and low soil moisture regimes. Seedling growth and physiology were evaluated periodically. Seedling survival was reduced when root damage reached levels of 60-80%. Root systems of all three species showed partial to total recovery by the end of the experiment. In general, root freezing damage caused reductions in seedling growth, with these reductions becoming less significant over time. Root damage had little to no effect on black spruce and jack pine seedling physiology, while white spruce CO 2 uptake decreased with increasing root damage. Shoot nitrogen content of all three species decreased slightly with increasing root damage.  相似文献   

13.
Contour hedgerows of multipurpose tree species in the sloping tea lands of Sri Lanka are expected to reduce soil erosion and also add significant amounts of plant nutrients to the soil via periodic prunings. The objective of this experiment was to characterize the biomass decomposition pattern and quantify the amount of nutrients added through prunings of six tree species (Calliandra calothyrsus, Senna spectabilis, Euphatorium innulifolium, Flemingia congesta, Gliricidia sepium and Tithonia diversifolia) currently being used in hedgerows associated with tea. Withered leaf and stem prunings (50 g) were enclosed in 2-mm litter bags, placed at 5-cm depth and retrieved after one, three, six, nine and 12 weeks. Loss of initial dry weight, N, P and K was measured. Single exponential decay function adequately described both dry weight and nutrient loss. Tree species differed significantly in their rate of breakdown with decomposition constants (k) varying from 0.0299 to 0.2006 week−1 for leaves and from 0.0225 to 0.0633 week−1 for stems. Gliricidia showed the highest k for leaves with the rest in the following descending order: Senna > TithoniaEuphatorium > Calliandra > Flemingia. A similar pattern was observed for loss of all nutrients with Calliandra and Flemingia always having lower k values than the rest. Although N immobilization was not observed, immobilization of P and K was observed during the first week of incubation in some species, particularly in stem prunings. Annual biomass of prunings differed significantly between tree species in the following descending order: Calliandra > Senna > Flemingia > Tithonia > Gliricidia > Euphatorium. Calliandra added the greatest amount of nutrients annually to the soil with Euphatorium adding the least. Calliandra prunings provided the annual total K requirement and 49% of the N requirement of mature tea. However, none of the species provided more than 5% of the P requirement. It is concluded that among the tree species tested, Calliandra and Flemingia are the most suitable for contour hedgerows in tea plantations of this agroclimatic region because of their higher soil nutrient enrichment capacity and slower decomposition rates which would minimize leaching losses. This revised version was published online in June 2006 with corrections to the Cover Date.  相似文献   

14.

This study investigated the stand structure in pine, spruce and deciduous forests in the border district of Finland and Russia. A total of 46 mature forest stands was selected as pairs, the members of each pair being as similar as possible with respect to their forest site type, age, moisture and topography. The stands were then compared between the two countries by means of basal areas and number of stems. The proportions of dominating tree species were 2-12% lower, and correspondingly the proportions of secondary tree species higher, in Russian forests. The density of the forest stock was also higher in each forest type in Russia. The forests in the two countries differed most radically in terms of the abundance of dead trees. The amount was two to four times higher in Russian deciduous and spruce forests, and in pine forests the difference was 10-fold. The stand structures indicated that Russian coniferous stands, in particular, were more heterogeneous than intensively managed pine and spruce stands in Finland.  相似文献   

15.

The root collar diameter and the height:diameter ratio are of particular importance in container-grown seedlings where a high density in the containers may produce spindly seedlings. Temperature regimes and light quality are known to affect plant growth. The aim of this study was to identify responses in Picea abies (L.) Karst. seedlings grown with light providing different red:far-red ratios and under temperature regimes with alternating day (DT) and night temperature (NT) from negative (DT < NT) to positive (DT > NT) difference (DIF) between DT and NT. Experiments were conducted in controlled environment chambers and in a daylight phytotron. Only limited thermoperiodic responses appeared in P . abies seedlings with respect to seedling height and dry weight accumulation. The formation of terminal buds, however, was clearly delayed in seedlings grown at negative DIF. The results indicate a requirement for day extension light that is high in far-red, to prevent terminal bud formation under natural short-day conditions. An extended study should be conducted to clarify the minimum level of light intensity and the optimal light quality needed to prevent terminal bud formation under natural short-day conditions.  相似文献   

16.

The effects of seed weight and seed type on seedling growth of Pinus sylvestris (L.) were studied by seeding individually weighed orchard and stand seed in different mixtures under harsh (direct seeding in field) and optimal (seeding in nursery) conditions. In the nursery experiment an increase in the seed weight from 3 to 7 mg increased the seedling height by 10-27% and total weight by 27-113%, and decreased the height/diameter ratio by 5-6% after 2 yrs. With elimination of seed weight effects, orchard seedlings were 2% taller than stand seedlings in year 2. Without elimination of seed weight effects, orchard seedlings were 7-13% taller. In the field experiment an increase in the seed weight from 3 to 7 mg increased seedling height by 18-65%, stem volume by 81-274% and the number of top-buds by 23-34% in year 5. After elimination of seed weight effects, orchard seedlings were 7-13% taller than stand seedlings and without elimination of seed weight effects 20-21% taller after 5 yrs. Even after elimination of both seed weight and genetic effects orchard seedlings were 3-9% larger than stand seedlings in the field experiment. In conclusion, the influence of seed weight and seed type on growth traits and slenderness is highly significant and the influence seems to be greater in harsh conditions.  相似文献   

17.
本文分析了CAD在设计中引起的正面和负面影响,并进行了系统的阐述,从而使设计者在应用中能够保持客观的态度。  相似文献   

18.
Heterobasidion parviporum and Heterobasidion annosum are widely distributed root‐rot fungi that infect conifers throughout Europe. Infection of conifer stumps by spores of these pathogens can be controlled by treating fresh stumps with a competing non‐pathogenic fungus, Phlebiopsis gigantea. In this study, growth of three Latvian strains of P. gigantea and the biological control agent ‘Rotstop’ strain was evaluated in stem pieces of Norway spruce, Scots pine, lodgepole pine, Douglas‐fir, Weymouth pine, Siberian larch and Sitka spruce. The growth rates of one H. parviporum and one H. annosum isolate were also measured in the same stem pieces. The growth rate of P. gigantea varied greatly in wood of different conifer species. It was higher in the three pine species, lower in Norway spruce and lowest in Sitka spruce and Siberian larch, and in Douglas‐fir, this fungus did not grow. The largest area of wood occupied by P. gigantea was in lodgepole pine. Growth of Latvian isolates of P. gigantea in the wood of Pinus and Picea species was comparable to that of the Rotstop isolate. Consequently, stump treatment with local P. gigantea isolates should be recommended. However, our results suggest that Douglas‐fir stump treatment against Heterobasidion by P. gigantea may be ineffective and other stump treatment methods should be considered.  相似文献   

19.
Baobab leaves form an important part of the local diet in Sahel countries and elsewhere in Africa. Existing leaf nutritional data and agroforestry performance information are based solely on Adansonia digitata L., the baobab of continental Africa. The introduction potential of Adansonia species from the center of diversity in Madagascar and from Australia remains untapped. To assess this potential, the mineral contents and B1 and B2 vitamin levels of dried baobab leaves were determined for five-year old trees of A. digitata, A. gibbosa (A. Cunn.) Guymer ex D. Baum, A. rubrostipa Jum. & H. Perrier (syn. A. fony Baill.), A. perrieri Capuron and A. za Baill. grown in an introduction trial in Mali. Nutritional data were evaluated against survival and vigor to identify promising germplasm. Leaf vitamin and crude protein contents were highest in the Madagascar species, especially A. rubrostipa (B1 88 mg 100 g−1, B2 187 mg 100 g−1, protein 20.7% dry weight). However, the local species far outperformed the introductions in survival, tree height, basal diameter and resistance to termites. We suggest grafting as a way of harnessing the vigor of well-adapted local baobab varieties to the superior nutritional profiles of A. rubrostipa and others. Cross-species grafting tests in Adansonia were successful, thus creating new agroforestry possibilities with different scion/rootstock combinations.  相似文献   

20.
Abstract

Wood in general and wooden studs in particular are often distorted owing to uneven shrinkage during the drying process in the sawmill. Twist is often the most detrimental of all types of distortion, and it is caused by spiral grain in combination with variations in moisture content. For sawmills, the objective is to produce dried, straight boards, and one method of dealing with boards with excessive spiral grain is to sort them out and then dry them in a pretwisted position to obtain straight boards after drying. A model using the finite element (FE) method for the simulation of drying twist distortions was first calibrated against laboratory experiments in which boards were dried with and without restraints and pretwists. After the calibration, the FE results were compared with industrial test results for boards that were dried without restraints or with restraints with zero pretwist, i.e. straight restraints. The FE model used an elastic–ideally plastic material model to obtain permanent deformations. The calibration was to set the yield stresses so that there was a good match between FE results and results from the laboratory experiments. The comparison between the industrial test results and the FE results showed that the FE model is capable of realistic simulations of drying boards with and without restraints and presumably also pretwists.  相似文献   

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