超高效液相色谱-串联质谱法测定柑橘中的草甘膦及其代谢物残留     

张梦娜  杨云  王立平  潘兴鲁  徐军  吴小虎  王宽  董丰收  郑永权 《植物保护》2023,49(4):216-223

本研究首次建立了一种超高效液相色谱-串联质谱法(UHPLC-MS/MS)同时测定柑橘中草甘膦及其代谢物N-乙酰草甘膦?氨甲基磷酸(AMPA)和N-乙酰AMPA?样品经过0.5%甲酸水提取, 以十八烷基硅烷键合硅胶柱(C18)净化, 利用水和200 mmol/L碳酸氢铵溶液(含0.1%氨水)作为流动相梯度洗脱, 在多反应监测模式下定量分析?结果表明, 草甘膦及其代谢物在0.05~1 mg/kg范围内线性关系良好, 相关系数均大于0.99; 草甘膦及其3个代谢物在柑橘全果和果肉基质中3个加标水平下回收率为 70.5%~109.5%, 相对标准偏差(RSD)为0.6%~10.1%, 定量限为0.05 mg/kg?本方法的前处理样品无需衍生, 简便?快捷?高效?准确可靠, 可用于柑橘中草甘膦及其代谢物N-乙酰草甘膦?AMPA和N-乙酰AMPA的定量检测?  相似文献   

弱光条件下桃光合作用的动态变化及品种差异分析   总被引：3，自引：1，他引：3  

于桉  孔云  姚允聪 《中国农学通报》2005,21(9):242-248,254

就日光温室桃树光合生理进行了详尽的研究,结果表明:1d中叶温与气温以14:00时较高。遮阴明显地降低了到达叶片表面的有效光合辐射、叶温与气温。桃叶片的光合速率日变化为双峰曲线,峰值大约出现在上午10:00与下午14:00时;不同品种弱光下的光合速率有明显的差异,以NJN较高,其次为五月火与麦香。遮阴降低了桃叶片的光合速率,以NJN光合速率降低的较少,说明NJN能适应设施栽培。气孔阻力与蒸腾速率则随着遮阴程度的增加而增加。桃中位叶的光合速率较幼叶高。  相似文献   

Respond of Stock Trading Volume to Earning Report     

FU Yun ying  MENG Wei dong  CUI Di 《保鲜与加工》2002,(11):79-82

Earning report is a main accounting report that transmits earning information to users. It is the core of financial reports system. Earning information is significant to users' decision making. This paper studies the respond of stock trading volume to earning report and draws the curve of trading volume before and after earning report. This paper further does a regression analysis of accidental earning and abnormal return rate, and draws the relation curve of them on the earning report date to prove stock trading volume does have remarkable respond to earning report. This research is significant to either lessen small investors blindness investment and help them make reasonable forecast to markets and regulate the disclosure of listed companies.  相似文献   

Analysis on Sustained Release of Protein from Microcapsule Prepared by Alginate     

JIA Yun  DAI Chuan-yun  ZHAO Hong-wei  LIU Huo-an 《保鲜与加工》2005,(10):108-110

The paper studies a drug deliversy system for protein and find the optimum preparation condition.Cross-linked alginate(Alg) microcapsule was used to prepare microcapsule for protein,using bovine serum album(BSA) as a model drug.Effect of different cations and content of protein on configuration,size and enveloped rate of microcapsule were investigated.It is shown that Ba-Alg microcapsule has steady configuration,homogeneous size and high-enveloped rate.Also electrophoresis of native BSA before microencapsulation and after microencapsulation is measured by(SDS-PAGE),it is found that no significant change is observed BSA integrity.Release of BSA from microcapsule in vitro presents sustained release in some extent,and initial burst effect is significantly obvious.Microenpsulation drug in alginate will be a wishful drug delivery system.  相似文献   

Spline Boundary Element Method for Calculating Three-Dimensional Electrostatic Fields     

Yun Zhengqing Tan Bangding 《保鲜与加工》1993,(5):79-84

Based on [l].this paper presents a new spline-BEM for calculating 3-D electrostatic fields,in which bi-cubic B-splines are used as basis functions. The corner problem in BEM and the extreme conditions for splines are circumvented. The numerical results presented show that the global approximation .convergence and stability of the method are satisfactory.  相似文献   

Application OF SFRHSC IN Blast-Resistant Engineering     

JIAO Chu-jie  SUN Wei  GAO Pei-zheng  ZHOU Yun 《保鲜与加工》2007,(5):168-172

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The Application of Relevant Homology in the Unified Representation of Electromagnetic Potentials and Gauge Transformation     

Yun Zhengqing  Tan Bangding 《保鲜与加工》1995,(1):45-50

Electromagnetic potentials and gauge transformation are derived for non-cloSedexterior differential forms with the help of relevant homology.Since de Rham ccahomology is sure-ly a relavant homology. potentials for both closed and non-closed forms and the gauge transforma-tion ean be unified in terms of relavent homology.  相似文献   

The Unified Representation of Interface Conditionsof Electromagnetic Quantities Using Exterior Differential Forms     

Yun Zhengqing  Tan Bangding 《保鲜与加工》1994,(3):25-31

A continuity condition of p-forms across a p-dimensional submanifold isderived.The,various interface conditions of electromagnetic quantities are obtained through theapplication of the continuity condition to Minkowski manifold of space-time.  相似文献   

不同品种青贮玉米群体光合性能指标的变化     

张瑞霞  刘景辉  陈友君  朱树国  云丽娜  闫睿卿 《中国农学通报》2007,23(1):208-208

通过对不同青贮玉米品种群体光合性能指标的研究结果表明，不同青贮玉米品种叶面积指数、光合势、群体生长率在整个生育期均呈单峰曲线变化，峰值出现在散粉至乳熟期间，因不同品种而异。净同化率则呈“马鞍”型曲线变化。多分蘖品种科试1号、植株高大品种东陵白与农大647在生育期间叶面积指数和光合势均较高，东陵白生育前、中期群体生长率显著高于其它品种，且高值持续时间较长，这是其生物产量高的生理基础。生产中，采取合理栽培措施，克服此类品种植株高大、个体繁茂、群体郁蔽导致植株病害和倒伏严重的不足，可实现青贮玉米群体生物产量的进一步提高。  相似文献   

微波加热对米糠储藏性能和蛋白质溶解性的影响   总被引：3，自引：0，他引：3  

严梅荣  马云 《粮食储藏》2002,31(6):25-27

研究了微波加热对于米糠5周储藏期间酸值和过氧化值及米糠蛋白溶解性的影响。结果表明，利用微波加热稳定米糠，可以有效降低酸值，防止水解酸败，同时也能降低过氧化值。  相似文献