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Journal of Pest Science - Longhorn beetles are commonly moved among continents within wood packaging materials used in trades. Visual inspections carried out at points of entry often fail to detect...  相似文献   
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A gas chromatographic (GC) procedure is presented for the determination of residues of avilamycin and all its metabolites/conjugates which can be converted to the common moiety dichloroisoeverninic acid (DIA). The method involves alkaline hydrolysis to DIA, cleanup by partitioning with chloroform, acidification of the aqueous phase, and partitioning of DIA into methylene chloride. After methylation of DIA, the product, 3,5-dichloro-4,6-dimethoxy-2-methylbenzoic acid methyl ester, is cleaned up on a silica gel column prior to the final determination by electron capture GC. The method is sensitive to 0.1 mg/kg avilamycin equivalent. Overall average recoveries were 85.4%, with a standard deviation of 9.1% for n = 20. Analyses of feces, urine, tissues, and fat of pigs treated with avilamycin demonstrated that 93% of the administered substance is excreted in feces and urine, within 72 h after treatment, and that no residues (less than 0.01 mg/kg) can be found in the tissues and fat of the animals at any time between 0 and 7 days after treatment with medicated feed.  相似文献   
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Multiple cutaneous lymphosarcoma lesions in a 10-year-old German Shepherd regressed and totally healed by 5 weeks after cryotherapy of the larger lesions. The dog remains clinically normal 1 year after surgery, without use of corticosteroids or chemotherapy.  相似文献   
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