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Emel Alkan Fatih Kapukıran Elif Öztürk Er Dotse Selali Chormey Seyfullah Keyf Nizamettin Özdoğan Sezgin Bakırdere 《Water, air, and soil pollution》2018,229(9):298
The potential risk of pesticides to cause harm to humans and other organisms even at trace levels calls for sensitive and accurate analytical techniques for their simultaneous qualitative and quantitative determinations. In this study, a sensitive binary dispersive liquid-liquid microextraction (B-DLLME) strategy was developed for the simultaneous determination of phorate and oxyfluorfen by gas chromatography mass spectrometry after extraction/preconcentration from aqueous solution. An experimental design was used to optimize parameters of the B-DLLME method to obtain maximum outcome. Under the optimum conditions of B-DLLME, the limit of detection (LOD) for phorate and oxyfluorfen were found to be 0.41 μg L?1 and 0.54 μg L?1, respectively. The detection limits correlate to about 37 and 73 folds enhancement in detection powers when compared to direct GC-MS determination of phorate and oxyfluorfen, respectively. In order to find out the applicability of developed method to real samples, recovery tests were performed for 20 μg L?1 of phorate and oxyfluorfen spiked in well water samples. Percent recovery values were found to be 94.5% for phorate and 101.9% for oxyfluorfen. 相似文献
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M. Turan S. Ata A. Gunes N. Ataoglu A. Esringu O. Uzun M. Ozgul M. Y. Canbolat I. Bogdan 《农业科学与技术》2010,(6):20-33
The objective of this study was to DTPA （complexion agent） and a sequential extraction procedure, and adsorption-desorption isotherm （competitive） evaluate the mobility and distribution of Fe, Zn, Mn, Cu, Cd, Ni, and Pb using the in surface samples of five soil great groups differing in their physicochemical properties. For determining heavy metal adsorption and desorption capacities of soil samples, six different concentrations （0, 2.5, 5, 10, 15 and 20 mg Lt） were used in a laboratory experiment with tree replications. An analytical procedure involving sequential chemical extractions has been used for partitioning of heavy metals into five fractions. Sorption isotherms were characterized using linear, Frendlich and Langmuir equations. The results indicated that the selective sequences of the metal adsorption based on the distribution coefficient was Pb〉Cu〉Ni〉Cd〉Zn〉Mn〉Fe and Pb, Cu, and Ni are the most strongly sorbed metals by these soils, whereas Cd, Zn and Mn are the least sorbed ones. The total adsorbed amount of these metals on the studied soils was well described by Langmuir equation. Calciorthid had the highset Pb, Cu, Ni, Cd, Zn, Mn, and Fe adsorption, and the sequences followed order Fluvaquent〉Argiustoll〉Pellustert〉Haplustept of the studied soil. 相似文献
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Adem Güneş Nizamettin Ataoğlu Metin Turan Ahmet Eşitken Quirine M. Ketterings 《植物养料与土壤学杂志》2009,172(3):385-392
Phosphorus (P)‐solubilizing bacteria and fungi can increase soil‐P availability, potentially enhancing crop yield when P is limiting. We studied the effectiveness of Bacillus FS‐3 and Aspergillus FS9 in enhancing strawberry (Fragaria × ananasa cv. Fern) yield and mineral content of leaves and fruits on a P‐deficient calcareous Aridisol in Eastern Anatolia, Turkey. The 120 d pot experiment was conducted in three replicates with three treatments (Bacillus FS‐3, Aspergillus FS9, control) and five increasing rates of P addition (0, 50, 100, 150, and 200 kg P ha–1). Fruit yield and nutrient content of fruits and leaves and soil P pools were determined at the end of the experiment. Phosphorus‐fertilizer addition increased all soil P fractions. Strawberry yield increased with P addition (quadratic function) reaching a maximum of 94 g pot–1 at 200 kg P ha–1 in the absence of P‐solubilizing microorganisms. At this yield level, Bacillus FS‐3 and Aspergillus FS9 inoculation resulted in P‐fertilizer savings of 149 kg P ha–1 and 102 kg P ha–1, respectively. Both microorganisms increased yields beyond the maximum achievable yield with sole P‐fertilizer addition. Microorganism inoculation increased fruit and leaf nutrient concentrations (N, P, K, Ca, and Fe) with the largest increases upon addition of Bacillus FS‐3. We conclude that Bacillus FS‐3 and Aspergillus FS9 show great promise as yield‐enhancing soil amendments in P‐deficient calcareous soils of Turkey. However, moderate additions of P fertilizer (50–100 kg ha–1) are required for highest yield. 相似文献
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Metin Turan Quirine M. Ketterings Adem Gunes Nizamettin Ataoglu Aslihan Esringü Ali Volkan Bilgili 《Acta Agriculturae Scandinavica, Section B - Plant Soil Science》2013,63(5):427-436
Abstract Lucerne (Medicago sativa L.) is grown as a forage crop on many livestock farms. In calcareous soils in eastern Turkey, lucerne production requires boron (B) addition as the soils are naturally B deficient. Field experiments with four B-application rates (0, 1, 3, and 9 kg ha?1 B) were conducted in 2005 and 2006 to determine the optimum economic B rate (OEBR), critical soil test and tissue B values for dry matter (DM) production for lucerne grown on B-deficient calcareous aridisols in eastern Turkey. Boron application increased yield at each site in both years of production. The OEBR and critical soil and tissue B content were not impacted by location. Averaged over the two years and three locations, the OEBR was 6.8 kg B ha?1 with an average DM yield of 12.0 Mg ha?1. The average soil B content at the OEBR was 0.89 mg kg?1 while leaf and shoot tissue B content amounted to 51.8 and 35.5 mg kg?1, respectively. Boron application decreased tissue calcium (Ca), zinc (Zn), and copper (Cu), and increased tissue nitrogen (N), phosphorus (P), potassium (K), magnesium (Mg), iron (Fe), and manganese (Mn). Tissue and soil B increased without impacting yield at B levels up to 9 kg ha?1. We conclude that 7 kg ha?1 B is sufficient to elevate soil test B levels from 0.11 to 0.89 mg kg?1 and overcome B deficiency at each of the sites in the study. Similar studies with different soils and initial soil test B levels are needed to conclude if these critical soil and tissue values can be applied across the region. 相似文献
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