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为研究酒制熟地黄炮制工艺过程中梓醇的变化趋势和变化机理,利用HPLC检测酒制熟地黄炮制过程中不同时间点梓醇的含量,并利用FT-IR结合变温附件获取梓醇在不同温度点的红外光谱信息。结果表明,酒制熟地黄炮制过程中,梓醇含量整体呈下降趋势,但不同时间段梓醇含量下降率不同。梓醇含量下降的原因是其热稳定性较低,在温度90~100℃之间,其结构就发生变化。所以,生地黄产地加工焙干时,温度不能太高,以免梓醇含量下降;熟地黄炮制过程中,时间不能太短,以免“火候”不到。  相似文献   
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Qian XD  Wang XG  Zhong FY 《茶叶》2013,(4):491-492
Shengzhou is a major tea producing county in China and the major tea produced in Shengzhou is Yuexiang Longjing tea.Environment and tea cultivar are two important factors influencing tea quality.Chemical composition of tea samples prepared using materials from cultivars ‘Zhenong-117' and ‘ Baiye-1' were investigated.It showed that concentrations of total amino acids and catechins were more than 4.4% and 129 mg/g respectively,suggesting that Yuexiang Longjing had a good quality potential.  相似文献   
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An experiment was conducted to investigate the effect of plasma concentrations of the metabolic hormones [Growth hormone (GH), insulin and insulin‐like growth factor –I (IGF‐I)] and nutritional metabolites (Glucose, cholesterol, total protein, albumin, globulin, urea and creatinine) on the resumption of post‐partum ovarian activity in sixteen Friesian–Sanga cows grazing extensively on native grassland. Blood samples were taken from cows from week 1 to 16 post‐partum. Cows were classified as having resumed ovarian activity when a plasma progesterone concentration of ≥ 1.0 ng/ml was recorded for two consecutive weekly samples. Based on the resumption of ovarian activity, cows were classified as early‐cycling, late‐cycling or non‐cycling. The concentrations of the metabolic hormones were measured from week 1 to 10, while those of the nutritional metabolites were measured during week 1, 3, 5, 7 and 9 during the study period. The concentrations of the metabolic hormones, GH and insulin were similar (p > 0.05) in the three ovarian activity groups, likewise the concentrations of the nutritional metabolites, glucose, total protein, globulin, urea and creatinine. Plasma IGF‐I concentration was higher (p < 0.001) in early‐cycling (18.7 ± 0.74 ng/ml) than in late‐cycling (12.4 ± 0.75 ng/ml) and non‐cycling (10.4 ± 0.91 ng/ml) cows. Plasma cholesterol concentrations were significantly lower (p < 0.05) in early‐cycling (1.94 ± 0.15 mmol/l) compared with late‐cycling (2.48 ± 0.12 mmol/l) and non‐cycling (2.61 ± 0.11 mmol/l) cows. For plasma albumin concentrations, the levels recorded for early‐cycling cows were higher (40.7 ± 2.85 g/l) than in late‐cycling (34.4 ± 1.97 g/l) and non‐cycling (33.6 ± 2.66) cows. The results suggest that cows with lower plasma concentrations of IGF‐I and albumin, but higher plasma cholesterol concentrations were at risk of delayed resumption of post‐partum ovarian activity.  相似文献   
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