二甲硝咪唑盐的合成研究     

刘永琼  余红霞  邹军  李华枝 《中国兽药杂志》2001,35(4):23-25

本文报道以简便易行的方法合成水溶性二甲硝咪唑盐，收率高达95％以上，具工业化应用价值。  相似文献   

全乳固体微波滤纸快速测定方法的研究     

袁旭  柳智慧 《中国奶牛》2004,(3):51-53

将微波加热干燥技术和滤纸水分蒸发强化技术应用于全乳固体的快速测定．比较了该方法与GB5409-85减重法的差异和对乳中热敏物质乳糖稳定性的影响及测定结果的差异。经t检验得出了两种方法对乳糖的含量变化的差异不显著，全乳固体含量的测定结果相同，将测定时间由240min缩短至37min，可以满足生产对全乳固体快速测定的时间要求。  相似文献   

Changes in Endopeptidase Activity during Photosynthetic Declination in Rice Leaf     

DENG Zhi-rui ZHANG Rong-xian 《水稻科学》2004,11(1)

Two japonica rice varieties, Wuyujing 3 and 97-7, were used to study the changes in contents of soluble protein, free amino acids and endopeptidase activity during photosynthetic declination. The content of soluble protein in flag leaf of cv.Wuyujing 3 was higher than that of cv. 97-7, but decreased rapidly in Wuyujing 3. Free amino acids in flag leaf and the thirteenth leaf of Wuyujing 3 started to increase 10 days before the turning point of photosynthetic declination (TPPD), while it occurred just 1-2 days before TPPD in the flag leaf and the thirteenth leaf of 97-7. During reversible phase of photosynthetic declination,endopeptidase activity remained at a low level and increased slightly only in the later part of this phase. Then it rose up rapidly at irreversible decline phase and reached a very high level. For Wuyujing 3, the change in endopeptidase activity in the thirteenth leaf was parallel to that in flag leaf. However, for 97-7, the rapid increase of endopeptidase activity in the thirteenth leaf started later than that of flag leaf. The results implied that the rate of protein breakdown and conversion to transportable nitrogen in leaves of 97-7 was slower than that in leaves of Wuyujing 3 during photosynthetic declination and it led to relatively lower seed setting rate and fully filling grains rate in 97-7. This may be one of the important reasons why 97-7 could not bring the high yield potentiality into play and the findings may be taken into consideration while breeding for high potential varieties in future.  相似文献   

Physiological Basis of Irrigation Scheduling for Seed Production in Egyptian Clover Syn. Berseem (Trifolium alexandrinum L.) Crop     

N. C. Sinha  R. P. Singh 《Journal of Agronomy and Crop Science》1986,156(4):246-252

A field experiment was conducted to find out the critical physiological stages of irrigation schedules inducing better growth, physiological efficiency and seed yield potential of berseem ( Trifolium alexandrinum L., Var. S-99-1). For this purpose eight irrigation treatments were made comprised of four treatments of three irrigation (W₁, W₂, W₃ and W₄), three treatments of four irrigation (W₅, W₇ and W₈) and one treatment of five irrigation (W₆) at various physiological stages i. e. regeneration, flower initiation, full bloom, seed initiation and advance seed development stage.
Thus based on the experimental results the physiological role of watering in berseem seed production could be discussed as:
With-holding of irrigation either at regeneration or at full bloom stage developed potential water stress in plants as indicated by high proline content of irrigation treatments — W₄, W₁ and W₇; and further brought out disturbance on the formation of carotene, synthesis of water soluble sugar and translocation of sugar towards reproductive organs during grain development stage. These stresses adversely affected the plant growth and flowering behaviour. The irrigation at seed initiation stage increased the seed yield. Continuous irrigation did not appear to be useful. Thus it can be concluded that irrigation at three critical physiological stages i. e. regeneration, full bloom and seed initiation was found to be essential for obtaining potential seed yield of berseem.  相似文献   

测定石膏性盐渍土水溶性盐的适宜水土比     

戴祥韵  周斐德 《中国农业大学学报》1990,(1):55-58

土壤水溶性盐的含量与组成随制备浸出液的水土比例不同而异,对含石膏的盐渍土测定结果的影响尤为显著。为了正确反映田间水溶性盐的实际状况,作者进行了三种不同水土比例制备浸出液的对比试验。结果表明,适宜水土比为1:1,其测出的盐分含量与饱和泥浆法按近,且操作简便、快速,在我国一般土化分析实验室均可采用。  相似文献   

红汁乳菇多糖提取最佳工艺研究   总被引：10，自引：0，他引：10  

李志洲  杨海涛  邓百万 《中国食用菌》2003,22(5):40-42

对红汁乳菇多糖提取、纯化工艺进行了优化研究，结果表明在料液比1：30，浸提温度95％浸提时间2h,pH8．0，可获得最佳提取效果。在醇析浓度为70％，V(氯仿)：V(正丁醇)=1：0．2，V(氯仿 正丁醇)：V(样品)=1：l时，纯化含量为58％。同时用超声波法对红汁乳菇多糖的提取作了研究，其得率为6.99％，效果较佳。  相似文献   

高效液相色谱法测定氟甲喹可溶性粉含量   总被引：2，自引：0，他引：2  

王祖兵  程烨  吴梅芳 《中国兽药杂志》2004,38(12):20-22

采用高效液相色谱法测定氟甲喹可溶性粉的含量,采用C 18 色谱柱(150 mm×4.6 mm,5μm),以乙腈-水-磷酸(35∶65∶0.5,V/V)为流动相,柱温25 ℃,流速1.0 mL/min,检测波长248 nm.方法的线性范围 100～400 μg/mL,线性方程A=2.455×104C 28 111,r=0.999 9,平均回收率100.3%,RSD= 0.74%.本法具有专属性,可将氟甲喹与已知的杂质进行有效分离.  相似文献   

UHPLC-Q/TOF MS结合HPLC-DAD定性和定量分析硫酸黏菌素可溶性粉中的未知添加物     

陆春波  包爱情  周芷锦  张航俊  陈慧华 《中国兽药杂志》2018,52(12):54-60

定性和定量分析一批兽药硫酸黏菌素可溶性粉中的未知添加物。照《中国兽药典》2010年版一部对该批检品用微生物检定法进行含量测定时,发现该样品的抑菌圈为虚圈,用薄层色谱鉴别该样品,未显示与标准品溶液一致的主斑点,怀疑该样品中有处方外非法添加物。采用超高效液相色谱-四级杆-飞行时间质谱(UHPLC-Q/TOF MS)对该样品进行筛查,发现疑似添加物,并使用液相色谱-二极管阵列检测(HPLC-DAD)法进行了双重确证和含量测定。该样品中非法添加物确证为磺胺氯达嗪和甲氧苄啶,添加量分别为58.5 mg/g和13.4 mg/g。本研究通过建立筛查方法为监管部门提供技术支撑,通过分析非法添加物的可能原因为打击兽药处方外非法添加提供了思路。  相似文献   

Processing traits and digestibility of extruded dog foods with soy protein concentrate          下载免费PDF全文

K. S. Venturini  M. F. Sarcinelli  M. A. Baller  T. C. Putarov  E. B. Malheiros  A. C. Carciofi 《Journal of animal physiology and animal nutrition》2018,102(4):1077-1087

Soya bean protein concentrate (SPC) with two particle sizes were evaluated on extrusion parameters, kibble formation, digestibility and palatability of dog foods. Eight diets were extruded: PBM—control diet based on poultry by‐product meal (PBM); GM—a diet in which corn gluten meal (GM) replaced 45% of the diet protein; cSPC15%, cSPC30% and cSPC45%—diets in which SPC of coarse particle size (600 μm) replaced 15%, 30% and 45% of the diet protein; and sSPC15%, sSPC30% and sSPC45%—diets in which SPC of small particle size (200 μm) replaced 15%, 30% and 45% of the diet protein. The digestibility of nutrients was evaluated for the PBM, GM, cSPC45% and sSPC45% diets, using six dogs per food. The PBM, GM and cSPC45% diets were compared for palatability. Data were submitted for analysis of variance, and the means were compared by polynomial contrasts or Tukey's test (p < .05). The cSPC increased the specific mechanical energy (SME) application, extrusion temperature and pressure linearly, resulting in lower kibble density and higher expansion and starch gelatinization (SG) (p < .01). When comparing the PBM, GM, cSPC45% and sSPC45% diets, higher SME, extrusion temperature and pressure, SG and kibble expansion were verified for the cSPC45% diet (p < .05). The DM, fat and crude protein digestibility were similar among diets. Faecal pH, ammonia and lactate did not differ, demonstrating that the removal of oligosaccharides and soluble non‐starch polysaccharides of SPC produces an ingredient with mostly non‐fermentable fibre. Dogs preferred the PBM to the GM diet (p < .05), but consumed the PBM and cSPC45% foods equally. In conclusion, SPC exhibited good extrusion functionality, favouring kibble expansion and SG, with high digestibility, similar to that of PBM. The removal of soluble compounds from soya beans resulted in an ingredient with low fermentable fibre content, which did not alter faecal formation or characteristics.  相似文献   

Short‐term releases of CO2 from newly mixed biochar and calcareous soil          下载免费PDF全文

R. Cardelli  M. Becagli  F. Marchini  A. Saviozzi 《Soil Use and Management》2016,32(4):543-545

The work aimed to quantify native organic C mobilized in one calcareous soil in the 21 days after addition of biochar at a range of large to very large applications. The experiment was carried out in unplanted microcosms, and CO₂ flux was used as a measure of net mineralization. A rapid methodological approach, which does not require ¹³C as a tracer, was used to assess any priming effects induced by the biochar. The amount of CO₂‐C mobilized was small relative to the amount of biochar C and proportional to the amount of the biochar added. The additional CO₂‐C was similar to the content of the water‐soluble organic carbon in the biochar added with each application. No interaction with native soil C, that is priming effect, was observed.  相似文献