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原子光谱法测定水蜡树果中微量元素的含量
引用本文:于加平,常序,代春梅.原子光谱法测定水蜡树果中微量元素的含量[J].贵州农业科学,2009,37(12).
作者姓名:于加平  常序  代春梅
作者单位:1. 吉林农业科技学院,生物工程学院,吉林,吉林,132101
2. 吉林省吉林市卫生监督所,吉林,吉林,132100
摘    要:选用硝酸和高氯酸(5:1)混合消化液对水蜡树果进行消化,用火焰原子吸收光谱法测定水蜡树果中铁、锰、锌、铜的含量,原子荧光光谱法测定其中硒的含量.结果表明,水蜡树果中铁、锰、锌、铜、硒含量分别为86.65、19.33、23.80、12.11、0.037 μg/g,相对标准偏差0.75%~2.17%,回收率97.10%~103.28%.该方法快速、可行、精密度较好.

关 键 词:水蜡树果  微量元素  火焰原子吸收光谱法  原子荧光光谱法

Determination of Trace Elements Content in Fruits of Ligustrum obtusiifolium by Atomic Absorption Spectrometry
YU Jia-ping,CHANG Xu,DAI Chun-mei.Determination of Trace Elements Content in Fruits of Ligustrum obtusiifolium by Atomic Absorption Spectrometry[J].Guizhou Agricultural Sciences,2009,37(12).
Authors:YU Jia-ping  CHANG Xu  DAI Chun-mei
Abstract:The content of Fe, Mn, Zn, Cu and Se of Ligustrum obtusiifolium fruits digested by the mixed solution of HNO_3 and HClO_4(5:1) was determined by atomic absorption spectrometry and atomic fluorescence spectrometry. The results showed that the content of Fe, Mn, Zn, Cu and Se in fruits of Ligustrum obtusiifolium was 86.65 μg/g,19.33 μg/g, 23.80 μg/g,12.11 μg/g and 0.037 μg/g,their relative standard deviation was between 0.75% and 2.17% and their recovery was between 97.10% and 103.28%. The determination methods have the advantages of rapidity, feasibility and accuracy.
Keywords:Ligustrum obtusiifolium  trace element  atomic absorption spectrometry  atomic fluorescence spectrometry
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