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响应面法优化辣椒籽油碱异构化制备共轭亚油酸工艺及其氧化稳定性
引用本文:马燕,许铭强,李喜弟,孟新涛,邹淑萍,张婷,张谦.响应面法优化辣椒籽油碱异构化制备共轭亚油酸工艺及其氧化稳定性[J].新疆农业科学,2022,59(4):908-915.
作者姓名:马燕  许铭强  李喜弟  孟新涛  邹淑萍  张婷  张谦
作者单位:1.新疆农科院农产品贮藏加工研究所/新疆主要农副产品精深加工工程技术研究中心,乌鲁木齐 8300912.新疆西尔单食品有限公司,乌鲁木齐 830091
基金项目:农业部公益性行业科研专项“蔬菜副产物综合利用技术研究与示范”(201303079);农业部果蔬加工重点实验室开放基金项目“不同处理改性辣椒籽膳食纤维的特性研究”(GSKF2016003);新疆维吾尔自治区自然科学青年基金项目“超高压对辣椒籽蛋白特性的影响及其机理研究”(2016D01B031)
摘    要:目的]研究碱异构化法制备辣椒籽油共轭亚油酸工艺,得到高转化率的辣椒籽油共轭亚油酸,为辣椒副产物综合利用及制备共轭亚油酸的新资源开发提供理论依据.方法]以共轭亚油酸转化率为指标,以反应时间、反应温度、碱油比和溶油比为主要影响因素,运用响应面中心组合设计(CCD),分析不同因素对辣椒籽油共轭亚油酸转化率的影响,研究辣椒...

关 键 词:辣椒籽油  碱异构化  响应面优化  共轭亚油酸  氧化稳定性
收稿时间:2021-10-05

Optimization of Preparation of Conjugated Linoleic Acid by Alkali Isomerization of Pepper Seed Oil by Response Surface Methodology and Its Oxidation Stability
MA Yan,XU Mingqiang,LI Xidi,MENG Xintao,ZOU Shuping,ZHANG Ting,ZHANG Qian.Optimization of Preparation of Conjugated Linoleic Acid by Alkali Isomerization of Pepper Seed Oil by Response Surface Methodology and Its Oxidation Stability[J].Xinjiang Agricultural Sciences,2022,59(4):908-915.
Authors:MA Yan  XU Mingqiang  LI Xidi  MENG Xintao  ZOU Shuping  ZHANG Ting  ZHANG Qian
Institution:1. Institute of Farm Product Storage and Processing, Xinjiang Academy of Agricultural Sciences /Research Center of Xinjiang Main Farm Products Processing Engineering, Urumqi 830091,China2. Xinjiang Xierdan Food Co., Ltd., Urumqi 830091,China
Abstract:【Objective】 To study the preparation of conjugated linoleic acid from pepper seed oil by isomerization alkali in order to obtain high conversion of pepper seed oil conjugated linoleic acid.【Method】 The Conversion Rate of Conjugated Linoleic Acid was used as an indicator of investigation, the main influencing factors were reaction time, reaction temperature, alkali oil ratio and dissolved oil ratio, and the effects of different factors on conjugated linoleic acid conversion of pepper seed oil was analyzed by CCD. After that, the preparation process of conjugated linoleic acid from capsicum seed oil was determined, and the oxidation stability of conjugated linoleic acid between pepper seed oil and pepper seed oil was compared by Schaal oven accelerated test.【Result】 The optimal technical conditions are determined as follows by establishing the quadratic response regression model: The reaction temperature was 169℃, the reaction time was 4.4 h, Alkali oil ratio M(KOH):M (Pepper seed oil)] was 0.2, Dissolved oil ratio M(polyethylene glycol):M(Pepper seed oil)] was 1.7, and the conjugation conversion could reach 84.60%. Its oxidation stability was better than that of pepper seed oil.【Conclusion】 The process conditions of conjugated linoleic acid in pepper seed oil are optimized by response surface methodology, and the conjugated linoleic acid in pepper seed oil with good stability is obtained.
Keywords:pepper seed oil  response surface optimization  alkali isomerization  conjugated linoleic acid  oxidation stability  
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