| 热脱附-气相色谱/质谱分析菠萝果实香气研究 |
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| 引用本文： | 郑华,张汝国,于连松,张弘,马李一,王有琼.热脱附-气相色谱/质谱分析菠萝果实香气研究[J].广东农业科学,2009(5):122-123,149. |
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| 作者姓名： | 郑华 张汝国 于连松 张弘 马李一 王有琼 |
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| 作者单位： | 郑华,张汝国,张弘,马李一,王有琼(中国林业科学研究院资源昆虫研究所,云南昆明,650224);于连松(中国林业科学研究院资源昆虫研究所,云南昆明,650224;昆明理工大学化学工程学院,云南昆明,650224) |
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| 基金项目： | 国家科技支撑计划项目，国家林业局"948"项目 |
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| 摘 要： | 采用热脱附-气相色谱/质谱(TCT-GC/MS)联用技术,对动态顶空密闭循环吸附捕集的菠萝果皮及果肉的挥发物进行了检测,结果表明:菠萝果皮与果肉的香气中富含酯类化合物、尤其是甲酯类成分,含量最高的均为己酸甲酯、分别达到45.66%和64.45%;果皮挥发物中的2-甲基丁酸甲酯相对含量为8.03%、辛酸甲酯相对含量为6.44%,均比果肉中的含量(分别为6.50%和3.51%)高;果肉挥发物中未检出非酯类成分,而在果皮挥发物中检测到2,5-二乙烯基四氢吡喃(9.07%)和少量甲酸乙酸酐(0.87%).
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| 关 键 词： | 菠萝 挥发物 热脱附-气相色谱/质谱 分析 酯 |
Analysis on fragrances of pineapple by TCT-GC/MS |
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| ZHENG Hua ,ZHANG Ru-guo,YU Lian-song,ZHANG Hong,MA Li-yi,WANG You-qiong.Analysis on fragrances of pineapple by TCT-GC/MS[J].Guangdong Agricultural Sciences,2009(5):122-123,149. |
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| Authors: | ZHENG Hua ZHANG Ru-guo YU Lian-song ZHANG Hong MA Li-yi WANG You-qiong |
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| Institution: | ZHENG Hua 1,ZHANG Ru-guo1,YU Lian-song1,2,ZHANG Hong1,MA Li-yi1,WANG You-qiong1(1.Research Institute of Resources Insects,Chinese Academy of Forestry,Kunming 650224,China,2.Faculty of Chemical Engineering,Kunming University of Science and Technology,China) |
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| Abstract: | Fragrances from peel and inner-fruit of pineapple(Ananas comosus(L.) Merr.) were closely and circularly head-space sampled within adsorptive tubes,then analyzed by thermal-desorption cryo-trapping gas chromatography / mass spectrometry(TCT-GC/MS).Results showed that esters,especially methyl esters,were both high contained in the two samples.The contents of methyl caproate in peel(45.66%) and inner-fruit(64.45%) were both the highest among total volatile chemicals.In peel volatiles,the contents of butyric ac... |
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| Keywords: | Ananas comosus(L ) Merr volatile TCT-GC/MS anolysis ester |
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