| 炮制后安徽枳壳挥发性成分的GC-MS分析 |
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| 引用本文： | 彭金年,程庚金生,张付远,李丹丹.炮制后安徽枳壳挥发性成分的GC-MS分析[J].安徽农业科学,2014(34):12071-12072. |
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| 作者姓名： | 彭金年 程庚金生 张付远 李丹丹 |
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| 作者单位： | 1. 赣南医学院药学院,江西赣州,341000
2. 江西环境工程职业学院,江西赣州,341000 |
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| 摘 要： | 目的]建立气相色谱-质谱联用法（GC-MS）分析炮制后安徽枳壳中挥发性成分的方法.方法]采用顶空进样对样品中挥发性成分进行提取,运用气相色谱-质谱联用法对挥发性成分进行分离鉴定,以峰面积归一化法计算各挥发性组分的相对百分含量.结果]从炮制后安徽枳壳中分离出26种挥发性成分,鉴定出25个化学成分,其中主要成分是柠檬烯,占总挥发性成分的86.50％.结论]GC-MS适用于枳壳中挥发性成分的分析,可作为枳壳饮片质量评价的方法和依据.
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| 关 键 词： | GC-MS 安徽枳壳 挥发性成分 定性分析 |
Analysis of Volatile Components in Anhui Fructus Aurantii after Processing by GC-MS |
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| Institution: | PENG Jin-nian;CHENG Geng-jin-sheng;ZHANG Fu-yuan;College of Pharmacy,Gannan Medical University;Jiangxi Environmental Engineering Vocational College; |
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| Abstract: | Objective] The research aimed to establish a GC-MS method of analyzing volatile components in Anhui Fructus aurantii after processing.Method] The volatile components in Fructus aurantii obtained by headspace sampling were isolated and identified by GC-MS.The relative percentage of each volatile component was determined by area normalization method.Result] 26 compounds were isolated and 25 compounds were identified in Anhui Fructus aurantii and one of the main components was limonene,which was 86.50 percent of the total volatile components.Conclusion] GC-MS was suitable for analysis of volatile components from Chinese medicine and this research provides certain scientific basis for the quality evaluation of Fructus aurantii pieces. |
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| Keywords: | GC-MS Fructus aurantii Volatile components Qualitative analysis |
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