| 慢呼抗口服液中黄芩甙的含量测定 |
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| 引用本文： | 潘晓影,李继昌,柳颖,彭玮,田美湛.慢呼抗口服液中黄芩甙的含量测定[J].东北农业大学学报,2008,39(1):104-106. |
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| 作者姓名： | 潘晓影 李继昌 柳颖 彭玮 田美湛 |
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| 作者单位： | 东北农业大学动物医学学院,哈尔滨,150030 |
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| 基金项目： | 黑龙江省博士后科研启动基金 |
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| 摘 要： | 采用美国Waters C18(4.6mm×150mm,5μm)色谱柱分离,以甲醇-水-冰醋酸(50:49:1)为流动相,流速为1mL·min-1,检测波长270nm为条件,建立高效液相色谱法测定慢呼抗口服液中黄芩甙的含量。结果表明,此方法线性关系良好(R=0.9995);平均回收率(n=6)99.06%,RSD=1.01%。该法简便、快捷、准确,可以作为慢呼抗口服液质量控制的有效方法。
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| 关 键 词： | 慢呼抗口服液 黄芩甙 含量测定 高效液相色谱 |
| 文章编号： | 1005-9369（2008）01-0104-03 |
| 收稿时间： | 2006-10-30 |
| 修稿时间： | 2006年10月30 |
Content determination of baicalin in Manhukang oral liquid |
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| PAN Xiaoying,LI Jichang,LIU Ying,PENG Wei,TIAN Meizhan.Content determination of baicalin in Manhukang oral liquid[J].Journal of Northeast Agricultural University,2008,39(1):104-106. |
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| Authors: | PAN Xiaoying LI Jichang LIU Ying PENG Wei TIAN Meizhan |
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| Abstract: | A HPLC method was established for the determination of caffeotannic acid in Manhukang oral liquid. American Waters C18 (4.6 mmá150 mm, 5 ×ìm,(c) was used, and the mobile phase consisted of colonial spirit-aquaefer-glacial acetic acid(50,o49,o1,(c), the flow rate was 1.0 mL·min,-1. The detection wave length was 270 nm. The result showed that the linear relationship of this method was well(R=0.9995,(c), and the average re-covery was 99.06% (RSD=1.01%, n=6). It can be concluded that the HPLC method is simple, rapid and accurate, and can be used for the quality control of Manhukang oral liquid. |
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| Keywords: | Manhukang oral liquid baicalin content determination HPLC |
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