| 含氟杀虫剂类农药的残留检测分析研究进展 |
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| 引用本文： | 王建芬,丁双阳,王晓琳.含氟杀虫剂类农药的残留检测分析研究进展[J].中国农学通报,2016,32(2):68-72. |
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| 作者姓名： | 王建芬 丁双阳 王晓琳 |
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| 作者单位： | (;1.北京市延庆县畜牧技术推广站,北京 102100；;2.中国农业大学动物医学院,北京 100129；;3.河南牧业经济学院,郑州 450046） |
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| 基金项目： | 农业部公益性行业（农业）科研专项经费项目“食品质量安全‘主动’控制技术”(201203069-2)；奶牛产业技术体系北京市创新团队项目。 |
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| 摘 要： | 由于氟原子所具有的特殊功效，近几十年来含氟类农药发展迅速。含氟杀虫剂主要包括拟除虫菊酯和苯甲酰脲中的含氟品种，以及氟虫腈、溴虫腈、茚虫威等杂环类化合物。本研究对含氟杀虫剂类农药的残留分析方法进行了综述，包括样品提取技术、净化技术及检测技术。样品净化技术包括固相萃取和液-液萃取，检测技术主要有气象色谱法、高效液相色谱法、气相色谱-质谱联用(GC-MS)和高效液相色谱-质谱联用(HPLC-MS)。最后从动物性食品安全的角度提出建议。
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| 关 键 词： | 农用地 农用地 质量等别 空间技术 经济耦合性 Moran散点图 |
| 收稿时间： | 2015/1/28 0:00:00 |
| 修稿时间： | 2015/11/30 0:00:00 |
Research Progress of Analytical and Detection Methods of Fluorine-containing Pesticides Residues |
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| Wang Jianfen,Ding Shuangyang and Wang Xiaolin.Research Progress of Analytical and Detection Methods of Fluorine-containing Pesticides Residues[J].Chinese Agricultural Science Bulletin,2016,32(2):68-72. |
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| Authors: | Wang Jianfen Ding Shuangyang and Wang Xiaolin |
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| Institution: | (;1.Beijing Yanqing Animal Husbandry Technology Extension Station, Beijing 102100;2.College of Veterinary Medicine, China Agricultural University, Beijing 100129;3.Henan University of Animal Husbandry and Economy, Zhengzhou 450046) |
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| Abstract: | Because of the special function of fluorine atom for organism, fluorine-containing pesticide has been developed quickly in recent decades. The major classes of fluorine-containing pesticides are pyrethroid, benzoylurea and heterocyclic compounds which include fipronil, chlorfenapyr, indoxacarb, etc. In this study, the development of residue analytical methods including extraction, purification and detection techniques of fluorine-containing pesticide was described in detail. The purification techniques included solid-phase extraction and liquid-liquid extraction, the detection techniques included gas chromatography (GC), high performance liquid chromatography (HPLC), GC-MS and HPLC-MS. Finally suggestions were put forward from the aspect of animal derived food safety. |
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| Keywords: | fluorine-containing pesticide residue sample preparation instrumental analysis |
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