HPLC法对苹果中多菌灵残留及其消解动态的测定 |
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作者姓名: | 郭瑞刚 范崇辉 赵政阳 梁 俊 |
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作者单位: | 西北农林科技大学园艺学院 陕西杨凌712100 |
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基金项目: | 国家科技攻关项目(2004BA516A10)。 |
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摘 要: | 通过试验,确定一种简洁有效的方法来测定苹果中多菌灵的残留量。试验表明,苹果样品中多菌灵添加回收率在86.2% ̄101.9%之间,最小检出量为1.5ng,满足测定要求。多菌灵在苹果果皮中的消解动态方程为C=5.528e-0.1224d,半衰期为5.65d,果心中的消解方程为C=1.330e-0.1573d,半衰期为4.41d,果肉中的消解方程为C=1.255e-0.2970d,半衰期为2.33d。
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关 键 词: | HPLC 多菌灵 苹果 残留量 |
Determination of the Residues of Carbendazim and Degradation Trends in Apple by HPLC |
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Authors: | Guo Ruigang Fan Chonghui Zhao Zhengyang Liang Jun |
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Institution: | (College of Horticulture, Northwest A & F University, Yangling Shaanxi 712100) |
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Abstract: | A compact and effective method for determination of the residues of Carbendazim in apple was confirmed through the experiment. The fortified recoveries of Carbendazim were 86.2%~101.9% in the apple sample and the detection limit was 1.5ng; it can meet the experiment request. The elimination equation of dynamic state of Carbendazim for the apple peel, apple core and apple pulp are C=5.528e-0.1224d,C=1.330e-0.1573d and C=1.255e-0.2970d, the half-life time are 5.65, 4.41 and 2.33 days. |
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Keywords: | HPLC Carbendazim Apple Pestcide residue |
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