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50%噻虫胺水分散粒剂分析方法研究
引用本文:吴进龙,Zhang zhiyi,李国平,Chen Tiechun.50%噻虫胺水分散粒剂分析方法研究[J].农药科学与管理,2008,29(1):8-11.
作者姓名:吴进龙  Zhang zhiyi  李国平  Chen Tiechun
作者单位:农业部农药检定所,北京,100026
摘    要:本文采用高效液相色谱法,以甲醇 0.05%H3PO4为流动相,使用以ZORBAX80AExtend-C18、5μm为填料的不锈钢柱和二极管阵列检测器,在265 nm波长下对试样进行分离和定量分析.结果表明噻虫胺的线性相关系数为0.999 7;标准偏差为0.38;变异系数为0.77%:平均回收率为99.6%.

关 键 词:噻虫胺  高效液相色谱
文章编号:1002-5480(2008)01-08-04
收稿时间:2007-09-26

Analytical Method of Clothianidin By HPLC
Wu Jinlong,Zhang zhiyi,Li Guoping,Chen Tiechun.Analytical Method of Clothianidin By HPLC[J].Pesticide Science and Administration,2008,29(1):8-11.
Authors:Wu Jinlong  Zhang zhiyi  Li Guoping  Chen Tiechun
Abstract:A method for separation and quantitative analysis of clothianidin by HPLC with methanol and 0.05%H3PO4 as mobile phase, ZORBAX80A Extend-C18 column and DAD at 265nm wavelength was described. The result showed that the linear correlation coefficient was 0.999 7, the standard deviation was 0.38, the variation coefficient was 0.77%, the average recovery was 99.6%.
Keywords:clothianidin  HPLC
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