| 狭叶十大功劳化学成分分析 |
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| 引用本文： | 张晓会.狭叶十大功劳化学成分分析[J].中国兽药杂志,2011,45(10):34-36. |
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| 作者姓名： | 张晓会 |
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| 作者单位： | 1. 国家兽用药品工程技术研究中心,河南洛阳,471003
2. 中国石油天然气股份有限公司长庆油田分公司,宁夏灵武,751408 |
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| 摘 要： | 用乙酸乙酯对狭叶十大功劳茎叶的乙醇提取物进行萃取,萃取液浓缩后经反复的硅胶柱、凝胶柱层析分离纯化得到5个化合物,并通过理化性质和TLC、1H NMR、13C NMR、MS分析,鉴定化合物结构分别为小檗碱（Ⅰ）、药根碱（Ⅱ）、5’-甲氧基大风子品D（Ⅲ）、木犀草素（Ⅳ）和β-谷甾醇（Ⅴ）。其中5’-甲氧基大风子品D（Ⅲ）为首次从该属植物中分离得到。
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| 关 键 词： | 狭叶十大功劳 化学成分 结构鉴定 |
| 收稿时间： | 7/7/2011 12:26:06 PM |
| 修稿时间： | 8/7/2011 12:00:00 AM |
Chemical constituents Analysis of Mahonia fortunei. |
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| FAN Li-bo,ZHANG Xiao-hui,LIU Xing-jin,LONG De-ying.Chemical constituents Analysis of Mahonia fortunei.[J].Chinese Journal of Veterinary Drug,2011,45(10):34-36. |
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| Authors: | FAN Li-bo ZHANG Xiao-hui LIU Xing-jin LONG De-ying |
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| Institution: | FAN Li-bo1,ZHANG Xiao-hui1,LIU Xing-jin1,LONG De-ying2(1.National Research Center For Veterinary Medicine,Luoyang,Henan 471003,China,2.Chanqing Oilfield Subcompany,PetroChina Company Limited,Lingwu,Ningxia 751408,China) |
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| Abstract: | Five compounds were isolated from ethyl acetate extraction from ethanol extraction of stems and leaves of Mahonia fortunei,and purified by silica-gel and sephadex column chromatography.The structures of the compounds were determined by physicochemical properties and spectrum analysis（TLC,1H NMR,13C NMR,MS）.Five compounds were identified as berberine（Ⅰ）,jatrorrhizine（Ⅱ）,5＇-Methoxyhydnocarpin-D（Ⅲ）,lutelin（Ⅳ） and β-sitosterol（Ⅴ）.5＇-Methoxyhydnocarpin-D（Ⅲ） was isolated and identified from this plant for the first time. |
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| Keywords: | Mahonia fortunei Chemical constituents Structure identification |
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