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碱解玉米芯制备阿魏酸和对香豆酸
引用本文:夏文静,李飞,常钰,蒋雅静,沈燕.碱解玉米芯制备阿魏酸和对香豆酸[J].安徽农业科学,2014(29):10302-10305.
作者姓名:夏文静  李飞  常钰  蒋雅静  沈燕
作者单位:南京师范大学泰州学院生物技术与化学工程学院,江苏泰州,225300
摘    要:目的]利用碱解农林废弃物制备阿魏酸和对香豆酸。方法]对4种农林废弃物(花生壳、玉米秸秆、小麦秸秆、玉米芯)进行比较,发现玉米芯最适合用于提取阿魏酸和对香豆酸。考察不同氢氧化钠浓度、固液比(玉米芯/碱液)、提取温度、提取时间对玉米芯中阿魏酸和对香豆酸提取量的影响。结果]提取玉米芯中阿魏酸的最佳工艺条件为:氢氧化钠浓度为0.5 mol/L,固液比(玉米芯/碱液)为1∶30 g/ml,提取温度为50℃,提取时间为2.5 h。在此条件下,阿魏酸的提取量最高为14.05 mg/g,对香豆酸的提取量为21.12 mg/g。结论]研究可为提高玉米芯的附加值利用提供依据。

关 键 词:阿魏酸  对香豆酸  玉米芯  碱水解

Production of Ferulic Acid and p-cumaric Acid from Corn Cob by Alkaline Hydrolysis
Institution:XIA Wen-jing, LI Fei, CHANG Yu et al ( School of Biotechnology and Chemical Eninnening, Taizhou College, Nanjing Normal Univer- sity, Taizhou, Jiangsu 225300)
Abstract:The ferulic acid and p-cumaric acid were produced from agricultural residues by alkaline hydrolysis. Method]Corn cob was found to be the best through the comparison of alkaline hydrolysis of peanut shell,cornstalk,wheat straw and corncob. Effects of different sodium hydroxide concentration,solid-liquid ratio,extraction temperature and time on ferulic acid; p-cumaric acid were investigated.Result]Optimal hydrolysis conditions(NaOH concentration of 0.5 mol/L,solid/liquid ratio of 1∶30 g/ml,hydrolysis temperature of 50 ℃,hydrolysis time of 2. 5 h) ensured the production of hydrolysates with relatively high contents of both ferulic acid(14. 05 mg /g) and p-coumaric acid(21. 12 mg /g). Conclusion]The study can provide basis for improving added value utilization of corn cob.
Keywords:Ferulic acid  p-cumaric acid  Corn cob  Alkaline hydrolysis
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