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消解罐消解—火焰原子吸收法测定鱼肉中的锌
引用本文:陈剑杰.消解罐消解—火焰原子吸收法测定鱼肉中的锌[J].畜牧与饲料科学,2012,33(10):6-7.
作者姓名:陈剑杰
作者单位:山西农业大学动物科技学院,山西太谷,030801
摘    要:目的]建立消解罐消解—火焰原子吸收法测定鱼肉中锌的方法。方法]样品经消解罐消解后,用火焰原子吸收法测定样品中锌浓度。结果]该方法在锌浓度为0~2.0mg/L范围有良好的线性关系,相关系数r=0.9997,检出限锌为0.002μg/mL,相对标准偏差为3.12%,回收率锌为95.0%~102.5%。结论]该方法具有简便、快速、准确等优点,可用于鱼肉中锌的定量检测。

关 键 词:消解罐消解  火焰原子吸收法  鱼肉  

Determination of Zn by Digestion Tank Digestion and Flame Atomic Absorption Spectrometry
CHEN Jian-jie.Determination of Zn by Digestion Tank Digestion and Flame Atomic Absorption Spectrometry[J].Animal Husbandry and Feed Science,2012,33(10):6-7.
Authors:CHEN Jian-jie
Institution:CHEN Jian-jie (College of Animal Science and Veterinary Medicine, Shanxi Agricultural University, Taigu 030801, China)
Abstract:Objective]To establish a determination method of Zn in fish by digestion tank digestion and flame atomic absorption spectrometry. Method]The fish was dissolved by digestion tank digestion, and then Zn in fish was determined by flame atomic absorption spectrometry. Result]This method had good linear relation when the concentration range of Zn was 0-2.0 mg/L, and the correlation coefficient was 0.999 7. The detection limit of Zn was 0.002mg/mL, with the relative standard deviation of 3.12%. The recovery of Zn was 95.0%-102.5%. Conclusion ]The method is simole, raoid and accurate, so it is suitable for the determination of Zn in fish.
Keywords:digestion tank digestion  flame atomic absorption spectrometry  fish  Zn
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