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混剂中乙蒜素和三唑酮的气相色谱分析方法
引用本文:李娜,李英菊,李玉霞,马国章,曲鹏晶.混剂中乙蒜素和三唑酮的气相色谱分析方法[J].农药科学与管理,2009,30(9):47-49.
作者姓名:李娜  李英菊  李玉霞  马国章  曲鹏晶
作者单位:1. 山西省化肥农药产品质量监督检验站,山西省应用化学研究所,山西,太原,030027;太原理工大学材料科学和工程学院,山西,太原,030024
2. 山西省化肥农药产品质量监督检验站,山西省应用化学研究所,山西,太原,030027
摘    要:本文介绍了采用OV-101为固定液的石英毛细管柱,邻苯二甲酸二乙酯为内标物,程序升温气相色谱法对混剂中乙蒜素和三唑酮同柱一次性分离、定性、定量。测得结果在一定范围内成良好的线性,相关系数分别为0.9999、0.9998;变异系数分别为0.51%、0.75%;平均回收率为99.6%、99.9%。

关 键 词:乙蒜素  三唑酮  气相色谱  分析

Ditermination of the Mixture of Tradimefon and Ethylicin
Li Na,Li Yingju,Li Yuxia,Ma Guozhang,Qu Pengjing.Ditermination of the Mixture of Tradimefon and Ethylicin[J].Pesticide Science and Administration,2009,30(9):47-49.
Authors:Li Na  Li Yingju  Li Yuxia  Ma Guozhang  Qu Pengjing
Institution:Shanxi Institute of Applied Chemistry;Shanxi Quality Supervision and Inspection Station of fertilizer and Pesticide Products;Taiyuan 030027;China
Abstract:A method for seperation and determination of ethylicin and tradimefon in the mixture by GC with OV-101 capillary column and diethyl phthalate as internal standard was established.The results showed that the coeffecients of variation were 0.51% and 0.75% , the average recoveries were 99.6% and 99.9%, the linear correlations coefficient were 0.999 9 and 0.999 8 respectively.
Keywords:Ethylicin  Tradimefon  GC  analysis  
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