| 水果中有机磷农药多残留快速检测方法的比较研究 |
| |
| 引用本文： | 张玉廷,郑虎哲,崔春兰,刘艳.水果中有机磷农药多残留快速检测方法的比较研究[J].安徽农业科学,2006,34(23):6233-6234. |
| |
| 作者姓名： | 张玉廷 郑虎哲 崔春兰 刘艳 |
| |
| 作者单位： | 辽宁农业职业技术学院,辽宁营口,115009 |
| |
| 摘 要： | 以丙酮、二氯甲烷以及乙腈等作为提取剂,比较了国标法和CDFA-MRSM法对水果中有机磷农药的提取效率和回收率,提取液用气相色谱仪-火焰光度检测器进行定性、定量分析。结果表明,采用国标法测定农药的平均回收率为82.3%~90.2%,变异系数为3%~9%;采用CDFA-MRSM法测定农药的平均回收率为79.3%~88.7%,变异系数为4%~11%。说明2种方法准确度与精密度较好,均符合农药残留量分析的基本要求。
|
| 关 键 词： | 农药多残留 气相色谱 有机磷农药 固相萃取 |
| 文章编号： | 0517-6611（2006）23-6233-02 |
| 收稿时间： | 09 9 2006 12:00AM |
| 修稿时间： | 2006-09-09 |
Comparison of CDFA-MRSM and GB/T 5009 Mthod in the Determination of Organophosphor Pesticides in Fruit |
| |
| ZHANG Yu-ting et al.Comparison of CDFA-MRSM and GB/T 5009 Mthod in the Determination of Organophosphor Pesticides in Fruit[J].Journal of Anhui Agricultural Sciences,2006,34(23):6233-6234. |
| |
| Authors: | ZHANG Yu-ting |
| |
| Institution: | Haoning Agricultural Vocation-Technical College, Yingkou, Liaoning 115009 |
| |
| Abstract: | A testing method of multiresidue for the analysis of organophosphor pesticides in fruit with different extraction techniques was developed.The method is based on GB/T 5009 and CDFA-MRSM(California Department of Food and Agency-Mulritesidue Screen Method).Residues were determined with gas chromatography and Flame Photometric Detection(FPD).In the result,the recoveries in fruit samples were among 82.3%～90.2% with relative C.V among 3%～9% in GB/T 5009 method,and the recoveries in fruits samples were among 79.3%～88.7% with relative C.V among 4%～11% in CDFA-MRSM method,respectively.Both these methods had good recurrence. |
| |
| Keywords: | Multiresidue Gas Chromatography Organophosphor pesticides Solid phase extraction |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
