| 微波辅助提取-HPLC法测定神秘果种子中齐墩果酸 |
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| 引用本文： | 卢圣楼,刘红,江虹,黄巨波,王杰,胡成豪.微波辅助提取-HPLC法测定神秘果种子中齐墩果酸[J].湖北农业科学,2012(4):816-819,830. |
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| 作者姓名： | 卢圣楼 刘红 江虹 黄巨波 王杰 胡成豪 |
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| 作者单位： | 海南师范大学化学与化工学院;海南南派实业有限公司 |
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| 基金项目： | 海南省社会发展专项(2010SF007);海口市重点科技计划项目(2010-086) |
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| 摘 要： | 通过微波辅助提取法与超声提取法的比较研究与优化,确定提取神秘果(Synsepalum dulcificumDaniell)种子中齐墩果酸的最佳工艺条件,采用HPLC法测定神秘果种子中齐墩果酸的含量。结果表明微波辅助提取法具有操作简单、提取时间短和提取率高等优点。
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| 关 键 词： | 神秘果(Synsepalum dulcificum Daniell) 微波辅助提取法 超声提取 高效液相色谱 齐墩果酸 |
Determination of Oieanolic Acid in the Seed of Synsepalum dulcificum by Microwave Assistant Extraction-High Performance Liquid Chromatography |
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| LU Sheng-lou,LIU Hong,JIANG Hong,HUANG Ju-bo,WANG Jie,HU Cheng-hao.Determination of Oieanolic Acid in the Seed of Synsepalum dulcificum by Microwave Assistant Extraction-High Performance Liquid Chromatography[J].Hubei Agricultural Sciences,2012(4):816-819,830. |
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| Authors: | LU Sheng-lou LIU Hong JIANG Hong HUANG Ju-bo WANG Jie HU Cheng-hao |
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| Institution: | 1.College of Chemistry and Chemical Engineering,Hainan Normal University,Haikou 571158,China; 2.Hainan South Industrial Co.,LTD.,Haikou 571100,China) |
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| Abstract: | The optimized extraction method of oieanolic acid in the seed of Synsepalum dulcificum Daniell was established by comparison of microwave assisted extraction and ultrasonic extraction,and then detected by HPLC.The results indicated that microwave assisted extraction was advantage in the yield,timesaving and efficiency. |
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| Keywords: | Synsepalum dulcificum Daniell microwave assisted extraction HPLC ultrasonic extraction oleanolic acid |
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