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柴胡皂苷硅胶柱层析分离方法的研究
引用本文:王春兰,郑柏松.柴胡皂苷硅胶柱层析分离方法的研究[J].吉林农业科技学院学报,2011(1):6-7,18.
作者姓名:王春兰  郑柏松
作者单位:吉林农业科技学院中药学院,吉林132101
摘    要:为探讨柴胡单体皂苷的分离条件,采用超声波提取,正丁醇萃取,硅胶GH柱层析分离,层析检测方法。结果表明乙酸乙酯:95%乙醇(8:2)分离出三个单体化合物,说明硅胶柱层析可用于柴胡皂苷的制备性分离。

关 键 词:柴胡皂苷  硅胶G  柱层析

Study on the Saikosaponin Separation Method with Silica Jel Column Chromatography
WANG Chunlan,ZHENG Baisong.Study on the Saikosaponin Separation Method with Silica Jel Column Chromatography[J].Journal Of Jilin Agricultural Science And Technology College,2011(1):6-7,18.
Authors:WANG Chunlan  ZHENG Baisong
Institution:(Jilin Agricultural Science and Technology College College of Chinese Traditional Medicine Science,Jilin 12101)
Abstract:In order to establish monomer saikosaponin separation conditions from bupleurum,uesd ultrasonic extraction,butanol extraction,silica gel column chromatography Gh and chromatography detection method.The result showed that three compounds were separated when the rate of ethyl acetate and 95% ethanol was 8:2,the silica gel chromatography could be used for the separation of saikosaponin.
Keywords:saikosaponin  silica gel G  column chromatography
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