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吡唑草胺原药高效液相色谱分析方法研究
引用本文:胡琴,吴进龙,李国平.吡唑草胺原药高效液相色谱分析方法研究[J].农药科学与管理,2009,30(1):14-17.
作者姓名:胡琴  吴进龙  李国平
作者单位:1. 甘肃省植保植检站,甘肃,兰州,730020
2. 农业部农药检定所,北京,100026
摘    要:本文采用高效液相色谱法,以甲醇+酸水(pH4)为流动相,使用以ZORABX SB—C18、5μm为填料的不锈钢柱和二极管阵列检测器,在275nm波长下对试样中的吡唑苹胺原药进行分离和定量分析。结果表明吡唑草胺的线性相关系数为0.9998;标准偏差为O.30;变异系数为0.30%;平均回收率为99.49%。

关 键 词:吡唑草胺  高效液相色谱

Analytical Method of Metazachlor By HPLC
Hu Qin,Wu Jinlong,Li Guoping.Analytical Method of Metazachlor By HPLC[J].Pesticide Science and Administration,2009,30(1):14-17.
Authors:Hu Qin  Wu Jinlong  Li Guoping
Institution:Plant Protection and Plant Quarantine Station of Gansu Province;Gansu;Lanzhou 730030; Institute for the Control of Agrochemicals;Ministry of Agriculture;Beijing 100026
Abstract:A method for separation and quantitative analysis of metazachlor by HPLC with methanoland acid water (pH=4) as mobile phase, ZORABX SB-C18 column and DAD at 205nm wavelength was described. The result showed that the linear correlation coefficient was 0.999 8, the standard deviation was 0.30, the variation coefficient was 0.32%, the average recovery was 99.49%.
Keywords:Metazachlor  HPLC  
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