| SPE-GC/MS法同时测定蔬菜中克百威和三羟基克百威残留 |
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| 引用本文： | 赖 勇,唐淑军,梁 幸,宋世文,戴睿臻.SPE-GC/MS法同时测定蔬菜中克百威和三羟基克百威残留[J].热带作物学报,2010,34(2):1-5. |
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| 作者姓名： | 赖 勇 唐淑军 梁 幸 宋世文 戴睿臻 |
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| 作者单位： | 深圳市宝安区无公害农添加质产品监督检验站;深圳市宝安区无公害农添加质产品监督检验站;深圳市宝安区无公害农添加质产品监督检验站;深圳市宝安区无公害农添加质产品监督检验站;深圳市宝安区无公害农添加质产品监督检验站 |
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| 摘 要： | 采用乙腈提取，经石墨化碳黑氨基复合柱净化，GC/MS测定，采用内标法定量，建立了蔬菜中克百威和三羟基克百威残留的SPE-GC/MS同时测定方法。克百威的添加质量分数为0.16、0.4、1.0 mg/kg，方法平均回收率为94.3%、99.1%、97.7%，变异系数在5.0%、4.7%、5.1%，检出限0.0016mg/kg；三羟基克百威添加质量数为0.16、0.4、1.0 mg/kg，方法平均回收率为96.3%、100. %、95.9%，变异系数4.0%、4.2%、8.7 %，检出限0.0012mg/kg。
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| 关 键 词： | SPE-GC/MS 克百威 3-羟基克百威 残留 蔬菜 |
Determination of Carbofuran and 3-Hydroxycarbofuran Residues in Vegetables by SPE-GC/MS |
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| LAI Yong,TANG Shujun,LIANG Xing,SONG Shiwen and DAI Ruizhen.Determination of Carbofuran and 3-Hydroxycarbofuran Residues in Vegetables by SPE-GC/MS[J].Chinese Journal of Tropical Crops,2010,34(2):1-5. |
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| Authors: | LAI Yong TANG Shujun LIANG Xing SONG Shiwen and DAI Ruizhen |
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| Institution: | Pollution-Free Agricultural Products Inspection Station of Bao'an District;Pollution-Free Agricultural Products Inspection Station of Bao'an District;Pollution-Free Agricultural Products Inspection Station of Bao'an District;Pollution-Free Agricultural Products Inspection Station of Bao'an District;Pollution-Free Agricultural Products Inspection Station of Bao'an District |
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