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超声波、微波及热水提取菊花总糖的比较
引用本文:宋可珂,陈红艳,宾银平,马斌.超声波、微波及热水提取菊花总糖的比较[J].林业科技开发,2011,25(1):96-99.
作者姓名:宋可珂  陈红艳  宾银平  马斌
作者单位:北京林业大学理学院,北京,100083
摘    要:研究了常规热水法、超声波、微波、超声波预处理-热水提取和超声波-微波联用5种方法提取菊花总糖的工艺。结合苯酚-硫酸显色法,以菊花总糖提取量为考察指标,采用SAS软件对5种方法的提取结果进行统计分析。结果表明:超声波-热水法、超声波-微波法与常规热水法相比,结果差异显著(P>0.05),提取率大于常规法;超声波法、微波法与常规热水法相比,提取率差异不显著(P<0.05),其中超声波-热水处理法提取率最高。在菊花质量为5 g,料液比(g/mL)为1∶25,超声波功率500 W,温度60℃的实验条件下,先用超声波预处理30 m in,再在85℃的热水中回流提取30 m in,菊花总糖得率最高达到9.86%,比热水法的提取率高1.94%。这种提取方式提取效率高,安全可靠。

关 键 词:菊花总糖  超声波  微波  热水提取

Study on comparison of extracting Chrysanthemum saccharides by the methods of ultrasonic, microwave and hot water
SONG Ke-ke,CHEN Hong-yan,BIN Yin-ping,MA Bin.Study on comparison of extracting Chrysanthemum saccharides by the methods of ultrasonic, microwave and hot water[J].China Forestry Science and Technology,2011,25(1):96-99.
Authors:SONG Ke-ke  CHEN Hong-yan  BIN Yin-ping  MA Bin
Institution:SONG Ke-ke,CHEN Hong-yan,BIN Yin-ping,MA Bin College of Science,Beijing Forestry University,Beijing 100083,China
Abstract:The five methods of hot water,ultrasonic,microwave,ultrasonic pretreatment-hot water and ultrasonic-microwave combination to extract polysaccharides from Chrysanthemum were studied.The content of polysaccharides in the Ch.was determined with the method of phenol-sulfuric acid,and the software of SAS was used to analyze the data.The results showed that: the extraction rates of Ch.saccharides by the ultrasonic pretreatment-hot water method and the ultrasonic-microwave method were remarkable higher than that b...
Keywords:Chrysanthemum saccharides  ultrasonic method  microwave method  hot water extraction  
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