| 微波辐射硫酸氢钠催化合成乙酸异戊酯研究 |
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| 引用本文： | 王淑敏,李静.微波辐射硫酸氢钠催化合成乙酸异戊酯研究[J].河南农业大学学报,2005,39(2):226-228. |
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| 作者姓名： | 王淑敏 李静 |
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| 作者单位： | 许昌学院化学系,河南,许昌,461000 |
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| 基金项目： | 河南省教育厅自然科学基金项目(2002500019) |
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| 摘 要： | 在微波辐射下,以NaHSO4·H2O作催化剂,4A分子筛作脱水剂,以冰醋酸和异戊醇为原料合成乙酸异戊酯.当微波辐射功率为255W,以0.1mol冰醋酸为基准,催化剂用量为0.3g,酸醇的摩尔比为1∶1.5,反应时间20min时,酯化率达99.2%.
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| 关 键 词： | 微波辐射 硫酸氢钠 乙酸异戊酯 |
| 文章编号： | 1000-2340(2005)02-0226-03 |
Study on Synthesis of Isoamyl Acetate Catyzed by Sodium Bisulfate under Microwave Rradiation |
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| WANG Shu-min,LI Jing.Study on Synthesis of Isoamyl Acetate Catyzed by Sodium Bisulfate under Microwave Rradiation[J].Journal of Henan Agricultural University,2005,39(2):226-228. |
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| Authors: | WANG Shu-min LI Jing |
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| Abstract: | The synthesis of isoamyl acetate from acetic acid and isoamyl alcohol using sodium bisulfate as catalyst and 4 A molecular sieve as dehydrator is reported under microwave radiation.When the power of microwave radiation is 255 W , amount of catalyst 0.3 g (using 0.1 mol of acetic acid ) and reaction time 20 min, the conversion rate for acetic acid is 99.2%. |
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| Keywords: | microwave radiation sodium bisulfate isoamyl acetate |
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