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| 高效液相色谱-串联质谱法测定鸡肉中癸氧喹酯的测量不确定度评定 | |
| 引用本文： | 陈瑞清,俞道进,陈锋,黄一帆,江秀红.高效液相色谱-串联质谱法测定鸡肉中癸氧喹酯的测量不确定度评定[J].中国兽药杂志,2011,45(4):20-23,38. |
| 作者姓名： | 陈瑞清 俞道进 陈锋 黄一帆 江秀红 |
| 作者单位： | 1. 福建农林大学动物科学学院,福州,350002;福建省农产品质量安全检验检测中心,福州,350003 2. 福建农林大学动物科学学院,福州,350002 3. 福建省农产品质量安全检验检测中心,福州,350003 |
| 摘 要： | 分析了影响应用高效液相色谱-串联质谱法测定鸡肉中癸氧喹酯残留量的测量不确定因素,并对各不确定度分量进行了量化计算,最终求得扩展不确定度为0.56μg/kg,分析表明重复测量、制备标准溶液及内标溶液引入的不确定度分量是影响癸氧喹酯残留量测量不确定度的主要因素。 |
| 关 键 词： | 高效液相色谱-串联质谱 癸氧喹酯 鸡肉 测量不确定度 |
Evaluation on the Uncertainty of Measurement for the Determination of Decoquinate in Chicken by HPLC-MS/MS |
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| CHEN Rui-qing,YU Dao-jin,CHEN Feng,HUANG Yi-fan,JIANG Xiu-hong.Evaluation on the Uncertainty of Measurement for the Determination of Decoquinate in Chicken by HPLC-MS/MS[J].Chinese Journal of Veterinary Drug,2011,45(4):20-23,38. | |
| Authors: | CHEN Rui-qing YU Dao-jin CHEN Feng HUANG Yi-fan JIANG Xiu-hong |
| Institution: | 1.College of Animal Science,Fujian Agriculture and Forestry University,Fuzhou 350002;2.Fujian Inspection and Testing Centre for Agricultural Product Quality and Safety,Fuzhou 350003;China) |
| Abstract: | The impact factors in the evaluation on the uncertainty of measurement for the determination of decoquinate in chicken meat by high performance liquid chromatography-tandem mass spectrometry（HPLC-MS/MS） was analysed and evaluated.The expanded uncertainty was 0.56 μg/kg.The results showed that measurement repeatability,the preparation of standard solution and internal solution were the main factors in the evaluation on the uncertainty of measurement for the determination of decoquinate in chicken meat. |
| Keywords: | HPLC-MS/MS decoquinate chicken the uncertainty of measurement |
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