| 离子液体[BPY]BF4中4,6-二芳基嘧啶-2(1H)-酮的合成 |
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| 引用本文： | 陆蕾蕾,苑睿,林伟,吴翠,宛瑜.离子液体[BPY]BF4中4,6-二芳基嘧啶-2(1H)-酮的合成[J].西南农业大学学报,2011,33(1). |
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| 作者姓名： | 陆蕾蕾 苑睿 林伟 吴翠 宛瑜 |
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| 作者单位： | 江阴职业技术学院化学纺织工程系;江苏省药用植物生物技术重点实验室; |
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| 基金项目： | 国家自然科学基金资助项目(20772103); 江苏省高校自然科学重大基础研究资助项目(10KJA430050); 徐州师范大学自然科学基金资助项目(09XLA17,2010YLA003) |
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| 摘 要： | 在催化量浓盐酸催化下,以离子液体BPY]BF4为溶剂,以易得的芳香醛、芳香酮、尿素为原料,采用三组份一锅法合成了一系列4,6-二芳基嘧啶-2(1H)-酮类化合物,通过IR,1H NMR和13C NMR对产物进行了结构表征,为这类化合物提供了简便高效的绿色合成方法.
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| 关 键 词： | 离子液体 4 6-二芳基嘧啶-2(1H)-酮 合成 |
Synthesis of 4,6-Diarlymetadiazine-2(1H)-one in Ionic Liquid [BPY]BF4 |
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| LU Lei-lei,YUAN Rui,LIN Wei,WU Hui,WAN Yu.Synthesis of 4,6-Diarlymetadiazine-2(1H)-one in Ionic Liquid [BPY]BF4[J].Journal of Southwest Agricultural University,2011,33(1). |
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| Authors: | LU Lei-lei YUAN Rui LIN Wei WU Hui WAN Yu |
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| Institution: | LU Lei-lei1,YUAN Rui2,LIN Wei2,WU Hui2,WAN Yu21.Department of Chemical and Textile Engineering,Jiangyin Polytechnic College,Jiangyin Jiangsu 214405,China,2.Key Laboratory of Biotechnology of Medical Plants of Jiangsu Province,Xuzhou Jiangsu 221116 |
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| Abstract: | A series of 4,6-diarlymetadiazine-2(1H)-ones were synthesized greenly by the one-pot reaction of aromatic aldehyde,aromatic ketone and urea in ionic liquid BPY]BF4 with the catalyst HCl,and the structures were characterized by IR,1H NMR and 13C NMR.Thus,an environmental-friendly and effective method,with mild conditions,is provided for the synthesis of arrays of such compounds. |
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| Keywords: | ionic liquid 4 6-diarlymetadiazine-2(1H)-one synthesis |
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