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从马尾松毛虫中制备高脱乙酰度壳聚糖的初步研究
引用本文:刘卫星,刘高强,魏美才.从马尾松毛虫中制备高脱乙酰度壳聚糖的初步研究[J].安徽农业科学,2006,34(12):2935-2936.
作者姓名:刘卫星  刘高强  魏美才
作者单位:1. 中南林业科技大学生命科学与技术学院,湖南,长沙,410004;浙江科技学院经济管理学院,浙江,杭州,310023
2. 中南林业科技大学生命科学与技术学院,湖南,长沙,410004
基金项目:中南林业科技大学校科研和校改项目
摘    要:采用酸碱法从马尾松毛虫蛹中制备壳聚糖,结果表明:马尾松毛虫蛹依次经盐酸脱矿物质、氢氧化钠脱有机物质、双氧水脱色处理后获得白色片状固体物甲壳素,其水分含量为3.32%,灰分为0.99%,脱乙酰度为92.54%,粘度为18.3MPa·s;由甲壳素制备壳聚糖的条件为NaOH浓度50%,处理时间5h,处理温度80℃;由甲壳素获得壳聚糖产品的产率为79.21%。

关 键 词:昆虫资源  马尾松毛虫  壳聚糖  脱乙酰度
文章编号:0517-6611(2006)12-2935-02
收稿时间:03 20 2006 12:00AM
修稿时间:2006-03-20

Preliminary Study on the Preparation of Chitosn with High Degree of Deacetylation from Pupa of Dendrolimus punctatus Walker
LIU Wei-xing et al.Preliminary Study on the Preparation of Chitosn with High Degree of Deacetylation from Pupa of Dendrolimus punctatus Walker[J].Journal of Anhui Agricultural Sciences,2006,34(12):2935-2936.
Authors:LIU Wei-xing
Abstract:The preparation of chitosan from pupa of Dendrolimus punctatus Walker was studied with the acid-alkali method. The results showed that the chitin from D punctatus was obtained based on the removal of minerals and organic materials with HCl and NaOH,respectively. For the preparation of chitosan,the condition was the follows: alkali concentration was 50 %,treatment time was 5 h and treatment temperature was 80 ℃. The obtained chitosan under the condition was white sheet solid. The water and ash content of the chitosan product was 3.32 % and 0.99 %,respectively. The degree of deacetylation of the product was 92.54 %,viscosity was 18.3 MPa·s and the yield was 79.21 %.
Keywords:Insect resources  Dendrolimus punctatus Walker  Chitosan  Degree of deacetylation
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