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魔芋葡甘聚糖/MgO纳米复合材料的制备与表征
引用本文:田大听,王丹,山曼.魔芋葡甘聚糖/MgO纳米复合材料的制备与表征[J].安徽农业科学,2008,36(12):4953-4955.
作者姓名:田大听  王丹  山曼
作者单位:湖北民族学院化学与环境工程学院,湖北恩施,445000
基金项目:湖北省教育厅自然科学重点项目(D200629003);湖北民族学院自然科学重大项目.
摘    要:目的]研究纳米复合材料的制备及表征,以期制备一种新型食品包装材料。方法]以魔芋葡甘聚糖(KGM)为基体,以纳米MgO为原料,采用共混法制得KGM/MgO纳米复合物。通过傅立叶红外光谱(FTIR)、热重分析(TG)、透射电镜(TEM)等手段对该复合物进行了表征。结果]FTIR表明,纳米MgO粒子对KGM分子中某些特征官能团的波数影响比较大,纳米MgO和KGM之间存在较强的相互作用。E电镜表明,纳米MgO在复合材料中的分散性较好。制备的KGM/MgO纳米复合材料的热稳定性高于KGM薄膜。纳米MgO的加入对复合膜的力学性能有所提高。结论]用共混法成功制得了KGM/MgO纳米复合材料,为制备新型食品包装材料提供技术支撑。

关 键 词:魔芋葡甘聚糖  纳米MgO  纳米复合材料  共混
文章编号:0517-6611(2008)12-04953-02
修稿时间:2008年2月25日

Preparation and Properties of Konjac Glucomannan/MgO Nanocomposites
TIAN Da-ting.Preparation and Properties of Konjac Glucomannan/MgO Nanocomposites[J].Journal of Anhui Agricultural Sciences,2008,36(12):4953-4955.
Authors:TIAN Da-ting
Abstract:Objective] The objective of the research was to study the preparation and characterization of Nanocomposites so as to prepare a new food wrapper.Method] With Konjac glucomannan(KGM) as a matrix and nanoparticles as raw material,KGM/MgO Nanocomposites was obtained by blending method.The nanocomposites were characterized by Fourier transform infrared spectra(FTIR),thermogravimetry(TG),and transmission electron microscopy(TEM).Result] FTIR determination showed that MgO nanocomposites had great effect on the wave number of some functional group characteristic in KGM molecule.There was a stronger interaction between MgO nanocomposites and KGM.TEM electron microscopy showed that MgO nanocomposites had good decentralization in composites.The thermostability of prepared KGM/ MgO nanocomposites was better than that of the KGM film.Addition of MgO increased the mechanical properties of the compound film.Conclusion] KGM/MgO nanocomposites was prepared successfully by blending method,which provided the technique support for preparing the new food wrapper.
Keywords:Konjac glucomannan(KGM)  Nano-MgO  Nanocomposites  Blending
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