隆昌麻鸭脏器中铜含量的测定研究 |
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引用本文: | 邱艳,刘凯.隆昌麻鸭脏器中铜含量的测定研究[J].安徽农业科学,2011,39(20):12212+12218-12212,12218. |
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作者姓名: | 邱艳 刘凯 |
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作者单位: | 内江师范学院化学化工学院,四川,内江,641112 |
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摘 要: | 目的]为隆昌麻鸭的开发及养殖提供基础数据。方法]研究5-Br-PADAP分光光度法测定铜含量的显色体系,并用于隆昌麻鸭脏器中铜含量的测定。结果]隆昌麻鸭脏器铜含量的线形范围为0~7.5μg/25 ml,回归方程为A=0.031 05C-0.0197,相关系数r=0.9991,加标回收率为97.5%~104.2%。隆昌麻鸭各脏器中铜含量的大小顺序为:肝脏〉心脏〉肾脏〉菌肝〉肺。结论]该方法操作简便、灵敏度高,可用于隆昌麻鸭脏器中铜含量的测定。
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关 键 词: | 2-[5-溴-(2-吡啶偶氮)]-5-二乙氨基苯酚 微乳液 分光光度法 铜 |
Study on the Determination of Cuprum Content in Viscuses of Longchang Sheldrake |
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Institution: | QIU Yan et al(School of Chemistry and Chemical Engineering,Neijiang Normal University,Neijiang,Sichuan 641112) |
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Abstract: | Objective] The research aimed to provide basic data for the development and culture of Longchang Sheldrake.Method] The chromogenic system for the determination of cuprum content by 5-Br-PADAP spectrophotometry was studied and it was applied in the determination of cuprum content in the viscera of Longchang Sheldrake.Result] The linear range of cuprum content in the viscera of Longchang Sheldrake was 0-7.5 μg/25 ml and its regression equation was A=0.031 05C-0.019 7(r=0.999 1).The addition recovery rate was 97.5-104.2%.The order of cuprum content in the viscera of Longchang Sheldrake was liver>heart>kidney>liver>lung.Conclusion] This method was simple and highly-sensitive and it can be used in the determination of cuprum content in the viscera of Longchang Sheldrake. |
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Keywords: | 2-[5-bromine-(2-pyridine-azo)]-5-diethylamine phenol Microemulsion Spectrophotometry Cuprum |
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