| 美柄牛肝菌子实体的化学成分研究 |
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| 引用本文： | 左伟,罗都强.美柄牛肝菌子实体的化学成分研究[J].安徽农业科学,2010,38(5):2356-2357,2361. |
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| 作者姓名： | 左伟 罗都强 |
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| 作者单位： | 河北大学生命科学学院,药物化学与分子诊断教育部重点实验室,河北保定,071002;河北大学生命科学学院,药物化学与分子诊断教育部重点实验室,河北保定,071002 |
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| 基金项目： | 国家自然科学基金项目(30671385) |
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| 摘 要： | 目的]系统阐述美柄牛肝菌的主要化学成分。方法]以美柄牛肝菌为试材,采用常规硅胶柱层析、制备薄层层析、高效液相色谱等方法分离鉴定美柄牛肝菌中的化合物及其结构。结果]从美柄牛肝菌中分离出了9个化合物,分别为O-Acetylcyclocalopin A,分子式为C17H22O7;Cyclocalopin,分子式为C15H20O6;Cyclopinol,分子式为C15H20O5;D-阿洛醇（D-allitol）,分子式为C6H14O6;3β-羟基-麦角甾醇-5,7,22-三烯,分子式为C28H44O;3β-羟基-5α,8α-过氧化麦角甾醇-6,22-二烯,分子式为C28H44O3;邻苯二甲酸二异丁酯,分子式为C16H22O4;Bis（2-ethylhexyl）phthalate,分子式为C24H38O4;Ergosta-7,22-dien-3β,5α,6α-triol（cerevisterol）,分子式为C28H46O3。通过经典波谱学分析和文献比对确定了它们的结构,其中包括3个倍半萜类化合物和3个甾体类化合物,3个倍半萜类化合物仅对黄瓜枯萎病菌、小麦赤霉病菌等少数病原菌有微弱的抗菌作用。结论]该研究为利用美柄牛肝菌开发生物农药奠定了基础。
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| 关 键 词： | 化学成分 制备薄层层析 倍半萜 美柄牛肝菌 |
Research on the Chemical Components of the Fruit Bodies of Boletus calopus |
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| ZUO Wei et al.Research on the Chemical Components of the Fruit Bodies of Boletus calopus[J].Journal of Anhui Agricultural Sciences,2010,38(5):2356-2357,2361. |
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| Authors: | ZUO Wei |
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| Institution: | College of Life Science;Key Laboratory of Medicinal Chemistry and Molecular Diagnosis of Ministry of Education;Hebei University;Baoding;Hebei 071002 |
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| Abstract: | Objective] The purpose was to expound the main chemical components of Boletus calopus systematically.Method] With B.calopus as tested material,the compounds were isolated from B.calopus and their structures were identified by using methods,such as conventional silica gel column chromatography,Pre-TLC and HPLC.Result] Nine compounds were isolated from B.calopus,they were O-Acetylcyclocalopin A with molecular formula being C17H22O7,Cyclocalopin with molecular formula being C15H20O6,Cyclopinol with molecula... |
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| Keywords: | Chemical components Pre-TLC Sesquiterpenes Boletus calopus |
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