| 除草剂氟烯草酸（戊酯）的合成研究 |
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| 引用本文： | 陆阳,陶京朝,周志莲.除草剂氟烯草酸（戊酯）的合成研究[J].农药科学与管理,2009,30(6):33-35. |
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| 作者姓名： | 陆阳 陶京朝 周志莲 |
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| 作者单位： | [1]信阳农专有机化学教研室,河南信阳464000 [2]郑州大学化学系,河南郑州450001 [3]河南科易集团新药研究开发中心,河南信阳464000 |
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| 摘 要： | 氟烯草酸（戊酯）是由日本住友化学公司于20世纪80年代开发的酞酰亚胺类除草剂，适用于防除大豆、玉米等作物的杂草。对大豆田中的一年生阔叶杂草具有很好的防除效果。对后茬作物没有影响。其药效好、用量少。化学名称为2-氯-5-（环己-1-烯-1，2-二甲酰亚氨基）-4-氟苯氧基1乙酸戊酯。
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| 关 键 词： | 氟烯草酸(戊酯) 合成 工艺 |
Synthesis of Novel herbicide Flumiclorac-pentyl |
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| Institution: | Lu Yang ,Tao Jingzhao,Zhou Zhilian(Office of Organic Chemistry, Xinyang Agriculture College, Xinyang 464000;Chemistry Department of Zhengzhou University, Zhengzhou 450001, China;New Drug Research and Development Center, Henan Keyi Group, Xinyang 464000) |
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| Abstract: | 2-chlorine-4-fluorine-5-nitrophenol was prepared from p-tludrophenol as starting material by the way of chlorination, esterification, nitrifacation, hydration.Flumiclorac-pentyl was synthesized using 2-chlorine-4-fluorine-5-nitropnenol as intermediate by the way of esterification, reduction, condensation.The recovery of this method was 55.42%, and the purity of the final product could be 98%. |
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| Keywords: | Flumiclorac-pentyl Synthesis preparation |
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