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Synthesis and characterization of nanocrystalline CoWO4@silk fibers with antibacterial activity under ultrasound irradiation
Authors:Azadeh Azadbakht  Amir Reza Abbasi  Nourolah Noori  Ezzat Rafiee  Mojtaba Taran
Institution:3687. Department of Chemistry, Faculty of Science, Khorramabad Branch, Islamic Azad University, Khorramabad, Iran
1687. Faculty of Chemistry, Razi University, Kermanshah, 67149, Iran
2687. Microbiology Laboratory, Biology Department, Razi University, Kermanshah, 67149, Iran
Abstract:The present investigation reports the novel synthesis of CoWO4 nanoparticles@silk fiber under ultrasound irradiation. The effect of temperature, power of ultrasound irradiation and sequential dipping steps in growth of the CoWO4 particles were studied. Results show a decrease in the particles size as the temperature and power of irradiation decreased. The fibers containing CoWO4 nanoparticles were tested for their antibacterial efficacy against E. coli and S. aureus and were found to possess significant antibacterial activity. The results show the CoWO4 nanoparticles@silk with strongest fluorescence characteristics can be obtained in this method. The physicochemical properties of the nanoparticles were determined by X-ray diffraction (XRD), scanning electron microscopy (SEM) and fluorescence spectroscopy.
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