| 气相色谱法测定稻谷中三环唑的不确定度分析 |
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| 引用本文： | 徐冲,李玉丹,赵立琴,刘远洋.气相色谱法测定稻谷中三环唑的不确定度分析[J].农产品加工．学刊,2019(9):36-38,42. |
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| 作者姓名： | 徐冲 李玉丹 赵立琴 刘远洋 |
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| 作者单位： | 黑龙江八一农垦大学测试中心;农业农村部农产加工品质量监督检验测试中心(大庆);黑龙江八一农垦大学生物技术中心;黑龙江八一农垦大学食品学院 |
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| 基金项目： | 大庆市指导性科技计划项目(ZD-2017-78) |
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| 摘 要： | 采用气相色谱法对稻谷中三环唑残留量的不确定度进行评估。根据JJF 1135—2005化学分析测量不确定度评定和JJF 1059.1—2012测量不确定度评定与表示中的相关规定,对测定过程中可能引入的不确定度进行分析和评估,建立了测定稻谷中三环唑残留量不确定度评定的数学模型,分析不确定度的主要来源,并将各分量进行合成。得出当稻谷中三环唑的量为0.262mg/kg时,其扩展不确定度为0.020 mg/kg (k=2)。
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| 关 键 词： | 不确定度 稻谷 三环唑 气相色谱法 评定 |
Evaluating Uncertainty of Determination of Tricyclazole in Rice in Husk by Gas Chromatography |
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| XU Chong,LI Yudan,ZHAO Liqin,LIU Yuanyang.Evaluating Uncertainty of Determination of Tricyclazole in Rice in Husk by Gas Chromatography[J].Nongchanpin Jlagong.Xuekan,2019(9):36-38,42. |
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| Authors: | XU Chong LI Yudan ZHAO Liqin LIU Yuanyang |
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| Institution: | (Testing Center,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China;Quality Supervision,Inspection and Test Center of Agricultural Processed Products(Daqing),Ministry of Agriculture and Rural Affairs,Daqing,Heilongjiang 163319,China;Biotechnology Center,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China;College of Food Science,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China) |
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| Abstract: | XU Chong;LI Yudan;ZHAO Liqin;LIU Yuanyang(Testing Center,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China;Quality Supervision,Inspection and Test Center of Agricultural Processed Products(Daqing),Ministry of Agriculture and Rural Affairs,Daqing,Heilongjiang 163319,China;Biotechnology Center,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China;College of Food Science,Heilongjiang Bayi Agricultural University,Daqing,Heilongjiang 163319,China) |
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| Keywords: | uncertainty rice in husk tricyclazole gas chromatography evaluation |
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