共查询到19条相似文献，搜索用时 203 毫秒
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建立乳与乳制品中香兰素、甲基香兰素、乙基香兰素和香豆素的反相高效液相色谱分析方法。用乙腈作为提取剂,氮吹浓缩,正己烷除脂净化,以C18反相色谱柱分离,20 mmol/L乙酸铵缓冲溶液（pH 5.6）-乙腈-甲醇为流动相,采用梯度方式洗脱,紫外检测波长267 nm,外标法定量。结果表明：4 种香兰素类化合物在0.05～5.00 μg/mL范围内线性良好,液态乳、乳粉、发酵乳、乳酸菌饮料、雪糕和干酪样品中香兰素、甲基香兰素、乙基香兰素和香豆素的定量限均为0.2 mg/kg,检出限均为0.06 mg/kg;液态乳、乳粉、发酵乳、乳酸菌饮料、雪糕和干酪中香兰素、甲基香兰素、乙基香兰素和香豆素添加量为0.2～2.0 mg/kg时,加标回收率分别为80.6%～110.0%、80.1%～109.6%、80.4%～109.5%、80.1%～105.9%,相对标准偏差分别为1.87%～7.70%、1.45%～9.80%、1.66%～9.52%、1.16%～9.52%。本方法快速、准确、重复性好、操作简便,适用于乳制品中香兰素、甲基香兰素、乙基香兰素和香豆素的含量测定。 相似文献
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淀粉酶值和羟甲基糠醛是判断蜂蜜质量的重要指标，淀粉酶值和羟甲基糠醛随着温度的升高时间的延长会发生一些较大的变化。淀粉酶值随着加热温度的升高、时间的延长呈下降的趋势，而羟甲基糠醛则随着加热温度的升高、时间的延长呈上升趋势，而且温度越高，上升速率越大。国家标准GB18796—2005规定淀粉酶值小于4和羟甲基糠醛含量大于40mg／kg的蜂蜜属于不合格产品，因此在生产加工和储存的过程中都应控制好温度及时间，以保证产品的质量，温度应控制在80℃以下。 相似文献
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韩刚 《广东畜牧兽医科技》1987,(3)
一、甜炼乳的质量和保存炼乳是一种浓缩乳制品饮料,它的种类有多种,按成品是否加糖、脱脂而有加糖炼乳(甜炼乳),不加糖炼乳(淡炼乳),全脂炼乳,脱脂炼乳及半脱脂炼乳。目前我国生产的炼乳,主要是甜炼乳和淡炼乳。甜炼乳就是在原料乳中加入约16％的蔗糖,并浓缩到原体积的40％左右的一种乳制品,成品中蔗糖含量为40～45％。甜炼乳的 相似文献
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为了探究后熟处理对蜂蜜品质的影响,本研究对送检的经不同后熟时间（0 h、12 h、36 h、48h和60 h）处理的五倍子蜂蜜进行主要品质指标（水分、淀粉酶活性、羟甲基糠醛、蔗糖、松二糖）的检测和分析。结果表明,五倍子蜂蜜中水分含量随着后熟时间的延长逐渐降低,后熟处理48 h后,五倍子蜂蜜中水分含量降至18.0%以下。松二糖、羟甲基糠醛、蔗糖和淀粉酶活性没有显著变化。经后熟处理60 h,最终包装成为成熟蜜后,五倍子蜂蜜中水分含量达15.9%,松二糖1.8%,淀粉酶活性15.4 mL/(g·h),蔗糖、羟甲基糠醛未检出,上述主要品质参数优于《GH/T 18796-2012蜂蜜》标准对蜂蜜一级品的要求;水分、松二糖、羟甲基糠醛等参数达到成熟蜂蜜要求。 相似文献
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为了了解广州市乳与乳制品的卫生质量状况,本文对市售的3000份乳与乳制品进行了微生物检测,发现液体乳,尤其是巴氏杀菌乳的合格率相对较低,不合格指标主要是菌落总数和大肠菌群数;婴幼儿配方乳粉也存在问题,其主要问题是阪崎肠杆菌和菌落总数超标;而干酪、炼乳、含乳饮料等的合格率较高。由此可见,控制微生物污染问题是确保乳与乳制品质量和安全的关键之一。 相似文献
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S. Iezzi A. Lifschitz J. Sallovitz P. Nejamkin M. Lloberas J. Manazza C. Lanusse F. Imperiale 《Journal of veterinary pharmacology and therapeutics》2014,37(6):589-594
Closantel (CLS) is currently used in programs for the strategic control of gastrointestinal nematodes. CLS is extralabel used in different dairy goat production systems. From available data in dairy cows, it can be concluded that residues of CLS persist in milk. The current work evaluated the concentration profiles of CLS in plasma and milk from lactating orally treated dairy goats to assess the residues pattern in dairy products such as cheese and ricotta. Six (6) female Saanen dairy goats were treated orally with CLS administered at 10 mg/kg. Blood and milk samples were collected between 0 and 36 days post‐treatment. The whole milk production was collected at 1, 4, 7, and 10 days post‐treatment to produce soft cheese and ricotta. CLS concentrations in plasma, milk, cheese, whey, and ricotta were determined by HPLC. The concentrations of CLS measured in plasma were higher than those measured in milk at all sampling times. However, the calculated withdrawal time for CLS in milk was between 39 and 43 days postadministration to dairy goats. CLS residual concentrations in cheese (between 0.93 and 1.8 μg/g) were higher than those measured in the milk used for its production. CLS concentrations in ricotta were sixfold higher than those in the milk and 20‐fold higher than those in the whey used for its production. The persistent and high residual concentrations of CLS in the milk and in the cheese and ricotta should be seriously considered before issuing any recommendation on the extralabel use of CLS in dairy goat farms. 相似文献
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以牛乳为原料，红曲霉为辅助发酵剂，制备霉菌成熟干酪，并对红曲霉干酪的理化性质、游离氨基酸、微观结构及挥发性风味物质进行研究。结果表明：使用红曲霉作为辅助发酵剂加工的干酪得率16.55%、蛋白质含量18.03%、脂肪含量33.40%、钙含量376.67 mg/100 g、水分含量44.47%、盐含量863.67 mg/100 g；在成熟过程中，pH值呈先下降后上升再逐渐稳定的趋势；由微观结构可知，红曲霉对成熟干酪内部结构影响显著；通过高效液相色谱法及气相色谱-质谱联用法，共鉴定出23 种游离氨基酸及32 种挥发性化合物，与对照组相比，在成熟期结束时，实验组干酪中的游离氨基酸含量显著提高，平均增加58.8 倍，挥发性化合物的种类与含量也存在显著变化。 相似文献
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柠条缩合单宁提取工艺优化 《畜牧与饲料科学》2022,43(5):29-32
[目的] 确定柠条缩合单宁最佳提取工艺。[方法] 以从内蒙古四子王旗采集的柠条为试验材料,利用超声辅助溶剂浸提法提取缩合单宁,利用磷钨钼酸显色法测定缩合单宁含量;应用单因素试验研究提取温度、提取时间、液料比、丙酮体积分数对柠条中缩合单宁提取量的影响。[结果] 随提取温度的增加,柠条缩合单宁提取量呈先升高后降低的趋势,当提取温度为60 ℃时,提取量最大,为34.24 mg/g;随提取时间的增加,柠条缩合单宁提取量呈先升高后降低的趋势,当提取时间为80 min时,提取量最大,为26.38 mg/g;随液料比的增加,柠条缩合单宁提取量呈先升高后降低的趋势,当液料比为30:1时,提取量最大,为25.34 mg/g;随丙酮体积分数的增加,柠条缩合单宁提取量呈先升高后降低的趋势,当丙酮体积分数为70%时,提取量最大,为30.61 mg/g。[结论] 提取柠条缩合单宁的最适温度为60 ℃,最适时间为80 min,最适液料比为30:1,最适丙酮体积分数为70%。 相似文献
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【目的】 探究水热回流法提取蛹虫草培养残基中活性成分虫草素的最佳工艺参数。【方法】 选取液料比、提取次数、提取温度、提取时间4个因素进行单因素试验和正交试验,并通过高效液相色谱法（HPLC）测定虫草素含量,确定水热回流法提取蛹虫草培养残基的最佳工艺参数。【结果】 方法学验证结果表明,蛹虫草培养残基中虫草素含量的HPLC测定方法精密度、重复性、稳定性相对标准偏差（RSD）均<2%,准确度RSD为2.64%,标准曲线线性相关性高。正交试验结果显示,影响水热回流法提取效果的因素依次为提取时间、提取次数、液料比、提取温度,其中提取时间和提取次数对提取物虫草素含量均有显著影响（P<0.05）,提取温度和液料比影响不明显（P>0.05）。单因素试验和正交试验结果表明,蛹虫草培养残基的最佳提取工艺参数为：液料比25：1、提取次数5次、提取温度70 ℃、提取时间60 min,该提取条件下测得蛹虫草培养残基中虫草素含量为1.48 mg/g。【结论】 采用本研究确定的水热回流法最佳工艺参数能有效提取蛹虫草培养基活性成分,且操作简单实用,提取物活性成分得率稳定,为后续蛹虫草培养残基产品开发提供参考依据。 相似文献
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Influence of the calf presence during milking on dairy performance,milk fatty acid composition,lipolysis and cheese composition in Salers cows during winter and grazing seasons 
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下载免费PDF全文 A. Cozma B. Martin C. Cirié I. Verdier‐Metz J. Agabriel A. Ferlay 《Journal of animal physiology and animal nutrition》2017,101(5):949-963
The milking of Salers cows requires the presence of the calf. The removal of the calf would simplify the milking routine, but it could also modify the milk yield and the milk and cheese composition. Therefore, the aim of this experiment was to evaluate the effect of calf presence during milking during sampling period (winter or grazing periods), on dairy performance, milk fatty acid (FA) composition, lipolysis and cheese yield and composition. Nine and 8 Salers lactating cows were milked in the presence (CP) or absence (CA) of their calves respectively. During winter, the cows were fed a hay‐based diet and then they only grazed a grassland pasture. Calf presence during milking increased milk yield and milk 16:0 concentration and decreased milk fat content and milk total odd‐ and branched‐chain FA (OBCFA) concentrations. Calf presence only increased initial lipolysis in milk collected during the winter season. Milk from CP cows compared to CA cows resulted in a lower cheese yield and ripened cheeses with lower fat content. Milk from the grazing season had lower saturated medium‐chain FA and OBCFA concentrations and higher 18:0, cis‐9‐18:1, trans‐11‐18:1 and cis‐9, trans‐11‐CLA concentrations than that from the winter season. Initial milk lipolysis was higher in the winter than in the grazing season. These variations could be due to seasonal changes in the basal diet. Furthermore, the effect of calf presence during milking on milk fat composition was lower than that on dairy performance, cheese yield and composition. Removing the calf during the milking of Salers cows seems feasible without a decrease in milked milk, and with a positive effect on cheese yield and fat content, under the condition that we are able to select cows having the capacity to be milked easily without the calf. 相似文献
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试验旨在研究果香味剂对奶牛乳腺上皮细胞培养液中乳成分含量及培养液风味的影响。试验选用自制的奶牛乳腺上皮细胞,设5个处理组,果香味剂的添加剂量分别为0、5、10、15和20μg/mL。结果表明：①当培养基中果香味剂添加量为15μg/mL时,乳腺上皮细胞培养液中总蛋白水平、甘油三酯及乳糖含量均达到最高,其中对脂肪含量影响显著（P〈0.05）,而对蛋白和乳糖含量影响不显著（P〉0.05）,之后呈下降趋势,说明果香味剂可能会诱导奶牛乳腺上皮细胞乳蛋白、乳脂和乳糖分泌水平的升高;②运用PT/GC-MS分析乳腺培养液中的风味成分,与对照组相比,各试验组中除具有原有乳腺培养液的风味外,还有乙酸异丁酯、乙酸异戊酯、丙酸异戊酯、丙酸戊酯、丁酸异丁酯、丁酸戊酯、丁酸乙酯、邻苯二甲酸二异丁酯等物质成分,而这些物质成分正好是果香味剂中进入到乳腺培养液中的风味物质,且当添加剂量为15μg/mL时,各物质成分含量为最高（P〈0.05）,之后呈下降趋势。果香味剂能显著影响奶牛乳腺上皮培养液中乳成分含量和风味。 相似文献
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胡勇 《青海畜牧兽医杂志》2009,39(1):12-14
以牦牛乳为原料,研究了Mozzarella奶酪的制作技术,采用四巴素三水平正交试验的方法,研究了不同量的凝乳酶、氯化钙、食盐以及发酵温度对Mozzarella奶酪成品的口感、色泽、质地的影响,确定了该产品生产的最佳生产条件。 相似文献